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CAS No. : | 921619-91-2 | MDL No. : | MFCD32667041 |
Formula : | C28H18O8 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | UMTUQDSLNCYCDQ-UHFFFAOYSA-N |
M.W : | 482.44 | Pubchem ID : | 101427665 |
Synonyms : |
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Signal Word: | Warning | Class: | |
Precautionary Statements: | P233-P260-P261-P264-P270-P271-P280-P301+P312-P302+P352-P304 | UN#: | |
Hazard Statements: | H302-H315-H319-H332-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With sodium hydroxide Heating; | ||
With sodium hydroxide; water Reflux; | ||
With water Solvolysis; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: K3PO4 / Pd(PPh3)4 / dioxane 2: aq. NaOH / Heating |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
72.6% | With HCl In 1,4-dioxane; water; N,N-dimethyl-formamide Cu(NO3)2*2.5H2O and ligand were mixed and dispersed in DMF-1,4-dioxane-H2O (2:1:1), aq. HCl was added and stirred in 85°C bath for 16 h; ppt. was filtered warm (50°C), washed with warm DMF and dried in air; elem. anal.; | |
With HCl In 1,4-dioxane; water; N,N-dimethyl-formamide High Pressure; mixed and dispersed in DMF/1,4-dioxane/H2O, blue-green slurry turned clear upon addition of 2 drops of aq. HCl, heated to 80°C for 12 h, kept at this temp. for 3 d; crystn., filtered at 50°C, washed sequentially by DMF/H2O and DMF, dried briefly in air; elem. anal.; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: HCl / water; N,N-dimethyl-formamide; 1,4-dioxane 2: neat (no solvent) | ||
Multi-step reaction with 3 steps 1: HCl / water; N,N-dimethyl-formamide; 1,4-dioxane 2: acetone 3: neat (no solvent) |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: HCl / water; N,N-dimethyl-formamide; 1,4-dioxane 2: acetone |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In water; acetic acid at 80℃; for 48h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In water; acetic acid at 80℃; for 48h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In water; acetic acid at 80℃; for 48h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In water; acetic acid at 80℃; for 48h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
45% | With sodium hydroxide In ethanol at 170℃; for 72h; High pressure; Autoclave; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
52% | With sodium hydroxide In ethanol at 170℃; for 72h; High pressure; Autoclave; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With hydrogenchloride In water; N,N-dimethyl-formamide |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With hydrogenchloride In dimethyl sulfoxide; N,N-dimethyl-formamide |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With hydrogenchloride In lithium hydroxide monohydrate; N,N-dimethyl-formamide |