Home Cart Sign in  
Chemical Structure| 924895-30-7 Chemical Structure| 924895-30-7

Structure of 924895-30-7

Chemical Structure| 924895-30-7

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 924895-30-7 ]

CAS No. :924895-30-7
Formula : C24H24B2O4
M.W : 398.07
SMILES Code : CC1(C)C2=C(C3=C1C=C(B(O)O)C=C3)C=C(C(C)(C)C4=C5C=CC(B(O)O)=C4)C5=C2
MDL No. :N/A

Safety of [ 924895-30-7 ]

Application In Synthesis of [ 924895-30-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 924895-30-7 ]

[ 924895-30-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 924895-30-7 ]
  • [ 2620-76-0 ]
  • [ 924895-26-1 ]
YieldReaction ConditionsOperation in experiment
80% With sodium carbonate;tetrakis(triphenylphosphine) palladium(0); In 1,2-dimethoxyethane; water; for 8h;Reflux; Inert atmosphere; (1-7) Synthesis of Compound (1); Into a 300 ml three-necked flask, 2.0 g (5.0 mmole) of Intermediate 6, 3.9 g (11 mmole) of <strong>[2620-76-0]2-(4-bromophenyl)-1-phenylbenzimidazole</strong>, 0.23 g (0.20 mmole) of tetrakis(triphenylphosphine)palladium(0), 50 ml of 1,2-dimethoxyethane and 15 ml (30 mmole) of a 2 M aqueous solution of sodium carbonate were placed under the stream of argon, and the resultant mixture was heated under the refluxing condition for 8 hours. After the reaction was completed, the organic layer was washed with water and dried with magnesium sulfate, and the solvent was removed by distillation using a rotary evaporator. The obtained crude crystals were washed with 50 ml of toluene and 100 ml of methanol, and 3.4 g of a light yellow powder substance was obtained. The obtained substance was identified to be Compound (1) by the measurement of the field desorption mass spectrum (FD-MS) (the yield: 80%).
 

Historical Records

Categories