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Chemistry
Organic Building Blocks
Amines
(3-Aminocyclohexyl)methanol
Chemistry
Organic Building Blocks
Amines
Alcohols Aliphatic Cyclic Hydrocarbons

[ CAS No. 925921-14-8 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 925921-14-8
Chemical Structure| 925921-14-8
Structure of 925921-14-8 * Storage: {[proInfo.prStorage]}
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Product Details of [ 925921-14-8 ]

CAS No. :925921-14-8 MDL No. :MFCD19207586
Formula : C7H15NO Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 129.20 Pubchem ID :-
Synonyms :

Safety of [ 925921-14-8 ]

Signal Word: Class:
Precautionary Statements: UN#:
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Application In Synthesis of [ 925921-14-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 925921-14-8 ]

[ 925921-14-8 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 16636-51-4 ]
  • [ 925921-14-8 ]
YieldReaction ConditionsOperation in experiment
With borane-THF; In tetrahydrofuran; at 20℃; for 74.0h;Heating / reflux; Synthesis of 4; To a solution of 3 (2.0 g, 14 mmol) in THF (31 mL) was added dropwise via addition funnel 1.0 M BH3-THF (42 mL, 42 mmol). The solution was stirred at room temperature for 72 h and refluxed for 2 h. The solution was cooled, diluted with methanol (70 mL) and concentrated under reduced pressure. The residue was dissolved in methanol (70 mL) and 2 N HCI (70 mL) and refluxed for 1 h. The solution was cooled and the pH adjusted to 14 with a 6 N aqueous sodium hydroxide solution. The solution was cooled and the pH was made basic with 6 N NaOH. The mixture was extracted with methylene chloride (3 x 500 mL) and the combined organic layers were dried over sodium sulfate, filtered through diatomaceous earth, EPO <DP n="100"/>and concentrated under reduced pressure to afford 4 (1.7 g) which was used without further purification or characterization.
Reference： [1]Patent: WO2007/18941,2007,A2 .Location in patent: Page/Page column 98-99
[2]Patent: US2015/5280,2015,A1
  • 2
  • [ 53084-60-9 ]
  • [ 7757-82-6 ]
  • [ 925921-14-8 ]
YieldReaction ConditionsOperation in experiment
200 mg With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 30℃; for 15h; LAH (107 mg, 2.8 mmol) was added portionwise to a solution of ethyl 3-aminocyclohexanecarboxylate (320 mg, 1.87 mmol) in THF (5 mL) at 0 C. and continued stirring at 25-30 C. for 15 h. The reaction mixture was quenched with aqueous saturated <strong>[7757-82-6]sodium sulphate</strong> solution, filtered the solid precipitate, washed the solid with THF; the filtrate collected was concentrated under reduced pressure to afford 200 mg of the title compound. MS (ESI): m/z 130 (M+H).
Reference： [1]Patent: US2015/5280,2015,A1 .Location in patent: Paragraph 1026 - 1028

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