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Chemical Structure| 93192-72-4 Chemical Structure| 93192-72-4

Structure of 93192-72-4

Chemical Structure| 93192-72-4

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Product Details of [ 93192-72-4 ]

CAS No. :93192-72-4
Formula : C9H11NS
M.W : 165.26
SMILES Code : NC1CCSC2=C1C=CC=C2
MDL No. :MFCD00297135

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Application In Synthesis of [ 93192-72-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 93192-72-4 ]

[ 93192-72-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 3528-17-4 ]
  • [ 93192-72-4 ]
YieldReaction ConditionsOperation in experiment
Thiochroman-4-amine. To a solution of thiochroman-4-one (1.6 g) in EtOH (100 ml) was added NH4OAc (8.2 g), the mixture was heated at 50 C for 35 minutes then cooled to room temperature and treated with Na(CN)BH4 (0.96 g). The mixture was stirred at room temperature for 64 hours and the reaction solvent was removed in vacuo. The residue was dissolved in EtOAc and washed 4 times with 4N HCl. The combined aqueous washes were made basic with 3N NaOH, then extracted 5 times with EtOAc. The combined organic layers were dried over Na2SO4 and concentrated to provide 1.4 g of the title compound.
 

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