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Type HazMat fee for 500 gram (Estimated)
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Chemical Structure| 934-28-1 Chemical Structure| 934-28-1

Structure of 934-28-1

Chemical Structure| 934-28-1

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Product Details of [ 934-28-1 ]

CAS No. :934-28-1
Formula : C8H12O2
M.W : 140.18
SMILES Code : O=C([C@@H]1[C@](C2)([H])CC[C@]2([H])C1)O
MDL No. :MFCD19238070

Safety of [ 934-28-1 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H315-H318-H335
Precautionary Statements:P261-P264-P271-P280-P302+P352-P304+P340-P305+P351+P338-P310-P332+P313-P362-P403+P233-P405-P501
Class:8
UN#:3265
Packing Group:

Application In Synthesis of [ 934-28-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 934-28-1 ]

[ 934-28-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 777-12-8 ]
  • [ 934-28-1 ]
  • C16H15F3N2OS [ No CAS ]
YieldReaction ConditionsOperation in experiment
General procedure: Carboxylic acid 3 (0.2 mmol, 1 equiv.) and HATU (0.2 mmol, 1 equiv.) were dissolved in 1 mL DCE in a one dram vial charged with a stir bar. DIPEA (0.1 mL, 0.6 mmol, 3 equiv.) was added and the resulting solution was stirred at RT for 10 minutes. Amine 2 (0.2 mmol, 1 equiv.) was added to the mixture. The reaction solution was heated to 45 °C and stirred overnight. Upon completion the reaction mixture was condensed and loaded onto a 60g C-18 cartridge and purified over a gradient of 5-95percent ACN/H2O. The fractions containing product were identified by LC-MS and condensed under vacuum to give the final product 4. The final product was characterized by NMR.
 

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