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chloro(1,5-cyclooctadiene)iridium(I) dimer[ No CAS ]
[ 93621-64-8 ]
[ 179675-65-1 ]
Yield
Reaction Conditions
Operation in experiment
In acetone byproducts: AgCl; inert atmosphere; refluxing metal complex with AgBF4 for 1 h, cooling toroom temp., filtration off of AgCl, addn. of diamine, stirring at room temp. for 1 h; pptn. on pentane addn., collection (filtration), washing (Et2O), recrystn. (CH2Cl2/pentane);