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Chemical Structure| 936498-09-8 Chemical Structure| 936498-09-8

Structure of 936498-09-8

Chemical Structure| 936498-09-8

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Product Details of [ 936498-09-8 ]

CAS No. :936498-09-8
Formula : C15H10BrN
M.W : 284.15
SMILES Code : BrC1=CC(C2=NC=CC3=C2C=CC=C3)=CC=C1
MDL No. :MFCD09749872

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Application In Synthesis of [ 936498-09-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 936498-09-8 ]

[ 936498-09-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 936498-09-8 ]
  • [ 654664-63-8 ]
  • C33H21N [ No CAS ]
YieldReaction ConditionsOperation in experiment
61.3% With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In tetrahydrofuran; at 80℃; for 6h;Inert atmosphere; Compound to the dried round flask A (5g, 17.5mmol) 1eq, triphenylene-2-yl Borough Nick Acid (10.47g, 38.5mmol), 2.2eq, tetrakis (triphenylphosphine) palladium (0) (0.4g , 0.2mmol) 0.02eq, 2M K2CO3into an 40ml then sufficiently filled with nitrogen was stirred for 6 hours at 80 put 100ml of anhydrous tetrahydrofuran.After cooling to room temperature and put in distilled water to terminate the reaction back extracted with dimethyl ether as distilled water, filtered and the organic layer was dried over anhydrous magnesium sulfate.Separating the resultant mixture was concentrated under reduced pressure the organic layer was filtered, the filtrate to the column layer with ethyl acetate and hexane to obtain the compound 14 (4.5g, 61.3%).
 

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