[ CAS No. 937-75-7 ]

Name: 937-75-7|7,7-Dimethylbicyclo[2.2.1]heptane-1-carboxylic acid|95%
Brand: Ambeed
SKU: A1105617
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3d Animation Molecule Structure of 937-75-7

Structure of 937-75-7 * Storage: {[proInfo.prStorage]}

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Quality Control of [ 937-75-7 ]

COA NMR CNMR HPLC LC-MS

Related Doc. of [ 937-75-7 ]

SDS

Alternatived Products of [ 937-75-7 ]

Product Details of [ 937-75-7 ]

CAS No. :	937-75-7	MDL No. :	MFCD18070924
Formula :	C₁₀H₁₆O₂	Boiling Point :	-
Linear Structure Formula :	-	InChI Key :	N/A
M.W :	168.23 g/mol	Pubchem ID :	-
Synonyms :

Calculated chemistry of of [ 937-75-7 ]

Physicochemical Properties

Num. heavy atoms :	12
Num. arom. heavy atoms :	0
Fraction Csp3 :	0.9
Num. rotatable bonds :	1
Num. H-bond acceptors :	2.0
Num. H-bond donors :	1.0
Molar Refractivity :	47.21
TPSA :	37.3 Å²

Pharmacokinetics

GI absorption :	High
BBB permeant :	Yes
P-gp substrate :	No
CYP1A2 inhibitor :	No
CYP2C19 inhibitor :	No
CYP2C9 inhibitor :	No
CYP2D6 inhibitor :	No
CYP3A4 inhibitor :	No
Log Kp (skin permeation) :	-5.64 cm/s

Lipophilicity

Log Po/w (iLOGP) :	1.84
Log Po/w (XLOGP3) :	2.37
Log Po/w (WLOGP) :	2.29
Log Po/w (MLOGP) :	2.19
Log Po/w (SILICOS-IT) :	2.08
Consensus Log Po/w :	2.15

Druglikeness

Lipinski :	0.0
Ghose :	None
Veber :	0.0
Egan :	0.0
Muegge :	1.0
Bioavailability Score :	0.85

Water Solubility

Log S (ESOL) :	-2.31
Solubility :	0.824 mg/ml ; 0.0049 mol/l
Class :	Soluble
Log S (Ali) :	-2.79
Solubility :	0.27 mg/ml ; 0.00161 mol/l
Class :	Soluble
Log S (SILICOS-IT) :	-1.71
Solubility :	3.3 mg/ml ; 0.0196 mol/l
Class :	Soluble

Medicinal Chemistry

PAINS :	0.0 alert
Brenk :	0.0 alert
Leadlikeness :	1.0
Synthetic accessibility :	3.16

Safety of [ 937-75-7 ]

Signal Word:	Warning	Class:
Precautionary Statements:	P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P330-P363-P501	UN#:
Hazard Statements:	H302-H312-H332	Packing Group:
GHS Pictogram:

Application In Synthesis of [ 937-75-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Downstream synthetic route of [ 937-75-7 ]

[ 937-75-7 ] Synthesis Path-Downstream 1~31

1
[ 937-75-7 ]
[ 35683-23-9 ]

Yield	Reaction Conditions	Operation in experiment
	With sodium azide; sulfuric acid
	With tris-(2-chloro-ethyl)-amine

Reference： [1]Kursanow; Witt [Zhurnal Obshchei Khimii, 1955, vol. 25, p. 2509,2511;engl.Ausg.S.2401]
[2]Beak,P. et al. [Journal of the American Chemical Society, 1969, vol. 91, p. 5073 - 5080]

2
[ 35122-25-9 ]
[ 937-75-7 ]

Reference： [1]Kwart; Null [Journal of the American Chemical Society, 1958, vol. 80, p. 248]

3
[ 464-78-8 ]
[ 937-75-7 ]

Yield	Reaction Conditions	Operation in experiment
	With potassium hydroxide; hydrazine hydrate; 2,2'-[1,2-ethanediylbis(oxy)]bisethanol
	With sodium hydroxide; hydrazine In ethylene glycol at 210℃;
	With potassium hydroxide; hydrazine hydrate In diethylene glycol at 205℃;

Reference： [1]Kursanow; Witt [Zhurnal Obshchei Khimii, 1955, vol. 25, p. 2509,2511;engl.Ausg.S.2401]
[2]Deno,N.C. et al. [Journal of the American Chemical Society, 1960, vol. 82, p. 4719 - 4723]
[3]Bunce,N.J.; Murray,N.G. [Tetrahedron, 1971, vol. 27, p. 5323 - 5335]

4
[ 56695-01-3 ]
[ 937-75-7 ]

Yield	Reaction Conditions	Operation in experiment
	With acetic acid; zinc

Reference： [1]Bredt; May [Chemiker-Zeitung, Chemische Apparatur, 1910, vol. 34, p. 65]

5
[ 99174-01-3 ]
[ 937-75-7 ]

Yield	Reaction Conditions	Operation in experiment
	With potassium hydroxide; palladium Hydrogenation;

Reference： [1]Kwart; Null [Journal of the American Chemical Society, 1958, vol. 80, p. 248]

6
bornane-10-nitrile [ No CAS ]
[ 937-75-7 ]

Yield	Reaction Conditions	Operation in experiment
	With sulfuric acid at 190℃; im Einschlussrohr;

Reference： [1]Lipp [Justus Liebigs Annalen der Chemie, 1913, vol. 402, p. 355]

7
[ 908094-01-9 ]
[ 937-75-7 ]
[ 124-40-3 ]
[ 76890-61-4 ]

Yield	Reaction Conditions	Operation in experiment
	(i) SOCl₂, (ii) /BRN= 102415/, (iii) aq. HCl, (iv) /BRN= 605257/; Multistep reaction;

Reference： [1]Current Patent Assignee: GLAXOSMITHKLINE PLC - FR2327766, 1977, B1 [Chem.Abstr., 1977, vol. 87, # 102022][Chem.Abstr., 1977, vol. 87, # 102022]

8
[ 908094-01-9 ]
[ 937-75-7 ]
[ 74-89-5 ]
1-(7,7-Dimethyl-bicyclo[2.2.1]hept-1-yl)-2-methylamino-ethanone [ No CAS ]

Yield	Reaction Conditions	Operation in experiment
	(i) SOCl₂, (ii) /BRN= 102415/, (iii) aq. HCl, (iv) /BRN= 741851/; Multistep reaction;

Reference： [1]Current Patent Assignee: GLAXOSMITHKLINE PLC - FR2327766, 1977, B1 [Chem.Abstr., 1977, vol. 87, # 102022][Chem.Abstr., 1977, vol. 87, # 102022]

9
[ 64-18-6 ]
[ 937-75-7 ]
[ 62579-38-8 ]

Yield	Reaction Conditions	Operation in experiment
	(i) aq. H₂SO₄, MeOH, (ii) LiAlH₄, Et₂O, (iii) SO₃; Multistep reaction;

Reference： [1]Fiorentino,M. et al. [Journal of the Chemical Society. Perkin transactions II, 1977, p. 87 - 93]

10
[ 937-75-7 ]
[ 22463-27-0 ]

Yield	Reaction Conditions	Operation in experiment
	With sulfuric acid; dihydrogen peroxide for 8h;

Reference： [1]Beak,P. et al. [Journal of the American Chemical Society, 1969, vol. 91, p. 5073 - 5080]

11
[ 937-75-7 ]
[ 933-27-7 ]

Yield	Reaction Conditions	Operation in experiment
	With potassium <i>tert</i>-butylate; iodine In benzene
	(i) AgNO₃, aq. NH₃, (ii) I₂, cyclohexane; Multistep reaction;

Reference： [1]Barton,D.H.R. et al. [Journal of the Chemical Society, 1965, p. 2438 - 2444]
[2]Bunce,N.J.; Murray,N.G. [Tetrahedron, 1971, vol. 27, p. 5323 - 5335]

12
[ 937-75-7 ]
[ 35122-23-7 ]

Yield	Reaction Conditions	Operation in experiment
	With lithium aluminium tetrahydride In diethyl ether

Reference： [1]Deno,N.C. et al. [Journal of the American Chemical Society, 1960, vol. 82, p. 4719 - 4723] Wnuk,T.A.; Kovacic,P. [Journal of the American Chemical Society, 1975, vol. 97, p. 5807 - 5810]

13
[ 937-75-7 ]
[ 5271-65-8 ]

Yield	Reaction Conditions	Operation in experiment
	With pyridine; thionyl chloride
	With thionyl chloride

Reference： [1]Deno,N.C. et al. [Journal of the American Chemical Society, 1960, vol. 82, p. 4719 - 4723]
[2]Pratt,D.G.; Rothstein,E. [Journal of the Chemical Society C: Organic, 1968, p. 2548 - 2554]

14
[ 937-75-7 ]
[ 110051-86-0 ]

Yield	Reaction Conditions	Operation in experiment
	With phosphorus pentoxide; <i>N</i>,<i>N</i>-dimethyl-aniline Heating;

Reference： [1]Deno,N.C. et al. [Journal of the American Chemical Society, 1960, vol. 82, p. 4719 - 4723]

15
[ 937-75-7 ]
[ 62612-65-1 ]

Yield	Reaction Conditions	Operation in experiment
	With ammonium peroxydisulfate; sulfuric acid; silver nitrate In acetonitrile

Reference： [1]Fiorentino,M. et al. [Journal of the Chemical Society. Perkin transactions II, 1977, p. 87 - 93]

Yield	Reaction Conditions	Operation in experiment
	Rk. mit Triphenylzinnbromid u. Benzylamin in CHCl3 (2 Std., 25grad) gibt Triphenylzinn-apocamphan-1-carboxylat;
	Rk. mit Triphenylzinnhydrid in sd. Heptan (20 Std.) gibt Triphenylzinn-apocamphan-1-carboxylat;
	Rk. mit Pb-Tetraacetat u. LiCl zu 1-Chlor-7,7-dimethyl-bicyclo<2.2.1>heptan;

	Rk.m. N,N-Dimethyl-anilin, P2O5, Δ --> 7,7-Dimethyl-bicyclo<2.2.1>heptan-carbonsaeure-(1)-anhydrid;
	40percent;

Yield	Reaction Conditions	Operation in experiment
	1-Apocamphanmethanol (11), CrO3, Eisessig;

Yield	Reaction Conditions	Operation in experiment
	With hydrogenchloride; amalgamated zinc; toluene

Yield	Reaction Conditions	Operation in experiment
	With sodium ethanolate at 170 - 180℃; im Rohr;

20
[ 56695-01-3 ]
[ 64-19-7 ]
[ 937-75-7 ]

Reference： [1]Bredt; May [Chemiker-Zeitung, Chemische Apparatur, 1910, vol. 34, p. 65]

21
[ 66275-41-0 ]
[ 937-75-7 ]

Yield	Reaction Conditions	Operation in experiment
	Multi-step reaction with 2 steps 1: zinc dust; concentrated glacial acetic acid; glacial acetic acid 2: sulfuric acid / 190 °C / im Einschlussrohr

Reference： [1]Lipp [Justus Liebigs Annalen der Chemie, 1913, vol. 402, p. 355]

22
[ 937-75-7 ]
[ 62612-64-0 ]

Yield	Reaction Conditions	Operation in experiment
	Multi-step reaction with 2 steps 1: (i) aq. H₂SO₄, MeOH, (ii) LiAlH₄, Et₂O, (iii) SO₃ 2: 4>2S₂O₈, aq. H₂SO₄, AgNO₃ / acetonitrile

Reference： [1]Fiorentino,M. et al. [Journal of the Chemical Society. Perkin transactions II, 1977, p. 87 - 93]

23
[ 937-75-7 ]
[ 76890-56-7 ]

Yield	Reaction Conditions	Operation in experiment
	Multi-step reaction with 2 steps 1: (i) SOCl₂, (ii) /BRN= 102415/, (iii) aq. HCl, (iv) /BRN= 741851/ 2: lithium aluminium tetrahydride

Reference： [1]Current Patent Assignee: GLAXOSMITHKLINE PLC - FR2327766, 1977, B1 [Chem.Abstr., 1977, vol. 87, # 102022][Chem.Abstr., 1977, vol. 87, # 102022]

24
[ 937-75-7 ]
2-Dimethylamino-1-(7,7-dimethyl-bicyclo[2.2.1]hept-1-yl)-ethanol [ No CAS ]

Yield	Reaction Conditions	Operation in experiment
	Multi-step reaction with 2 steps 1: (i) SOCl₂, (ii) /BRN= 102415/, (iii) aq. HCl, (iv) /BRN= 605257/ 2: lithium aluminium tetrahydride

Reference： [1]Current Patent Assignee: GLAXOSMITHKLINE PLC - FR2327766, 1977, B1 [Chem.Abstr., 1977, vol. 87, # 102022][Chem.Abstr., 1977, vol. 87, # 102022]

25
[ 937-75-7 ]
[ 108124-81-8 ]

Yield	Reaction Conditions	Operation in experiment
	Multi-step reaction with 2 steps 1: SOCl₂ 2: AlCl₃
	Multi-step reaction with 2 steps 1: SOCl₂, Py 2: AlCl₃

Reference： [1]Pratt,D.G.; Rothstein,E. [Journal of the Chemical Society C: Organic, 1968, p. 2548 - 2554]
[2]Deno,N.C. et al. [Journal of the American Chemical Society, 1960, vol. 82, p. 4719 - 4723]

26
[ 937-75-7 ]
[ 21890-84-6 ]

Yield	Reaction Conditions	Operation in experiment
	Multi-step reaction with 2 steps 1: SOCl₂ 2: AlCl₃
	Multi-step reaction with 2 steps 1: SOCl₂, Py 2: AlCl₃ / CS₂

27
camphor-10-sulfonic acid [ No CAS ]
[ 937-75-7 ]

Yield	Reaction Conditions	Operation in experiment
	Multi-step reaction with 4 steps 1: SOCl₂, CaCO₃ 2: TsCl, Py / dioxane 3: KMnO₄, aq. Na₂CO₃ / acetone 4: N₂H₄*H₂O, KOH / bis-(2-hydroxy-ethyl) ether / 205 °C

Reference： [1]Bunce,N.J.; Murray,N.G. [Tetrahedron, 1971, vol. 27, p. 5323 - 5335]

28
Campher-10-chlorsulfoxid [ No CAS ]
[ 937-75-7 ]

Yield	Reaction Conditions	Operation in experiment
	Multi-step reaction with 2 steps 1: KMnO₄, aq. Na₂CO₃ / acetone 2: N₂H₄*H₂O, KOH / bis-(2-hydroxy-ethyl) ether / 205 °C

Reference： [1]Bunce,N.J.; Murray,N.G. [Tetrahedron, 1971, vol. 27, p. 5323 - 5335]

29
[ 4552-50-5 ]
[ 937-75-7 ]

Yield	Reaction Conditions	Operation in experiment
	Multi-step reaction with 3 steps 1: TsCl, Py / dioxane 2: KMnO₄, aq. Na₂CO₃ / acetone 3: N₂H₄*H₂O, KOH / bis-(2-hydroxy-ethyl) ether / 205 °C

Reference： [1]Bunce,N.J.; Murray,N.G. [Tetrahedron, 1971, vol. 27, p. 5323 - 5335]

30
[ 937-75-7 ]
[ 13248-53-8 ]

Yield	Reaction Conditions	Operation in experiment
	Multi-step reaction with 3 steps 1: H₂SO₄, aq. H₂O₂ / 8 h 2: SOCl₂ 3: tetramethylurea, AgBF₄ / chlorobenzene
	Multi-step reaction with 3 steps 1: H₂SO₄, aq. H₂O₂ / 8 h 2: SOCl₂ 3: AgBF₄
	Multi-step reaction with 3 steps 1: H₂SO₄, aq. H₂O₂ / 8 h 2: nBuLi / tetrahydrofuran 3: AgBF₄ / chlorobenzene

Multi-step reaction with 3 steps 1: H₂SO₄, aq. H₂O₂ / 8 h 2: nBuLi / tetrahydrofuran 3: AgBF₄

Reference： [1]Beak,P. et al. [Journal of the American Chemical Society, 1969, vol. 91, p. 5073 - 5080]
[2]Beak,P. et al. [Journal of the American Chemical Society, 1969, vol. 91, p. 5073 - 5080]
[3]Beak,P. et al. [Journal of the American Chemical Society, 1969, vol. 91, p. 5073 - 5080]
[4]Beak,P. et al. [Journal of the American Chemical Society, 1969, vol. 91, p. 5073 - 5080]

31
[ 937-75-7 ]
[ 13248-52-7 ]

Yield	Reaction Conditions	Operation in experiment
	Multi-step reaction with 2 steps 1: H₂SO₄, aq. H₂O₂ / 8 h 2: nBuLi / tetrahydrofuran

Reference： [1]Beak,P. et al. [Journal of the American Chemical Society, 1969, vol. 91, p. 5073 - 5080]

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Code	Phrase
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Code	Phrase
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P220	Keep/Store away from clothing/combustible materials.
P221	Take any precaution to avoid mixing with combustibles
P222	Do not allow contact with air.
P223	Keep away from any possible contact with water, because of violent reaction and possible flash fire.
P230	Keep wetted
P231	Handle under inert gas.
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P233	Keep container tightly closed.
P234	Keep only in original container.
P235	Keep cool
P240	Ground/bond container and receiving equipment.
P241	Use explosion-proof electrical/ventilating/lighting/equipment.
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P260	Do not breathe dust/fume/gas/mist/vapours/spray.
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Code	Phrase
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P305	IF IN EYES:
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P310	Immediately call a POISON CENTER or doctor/physician.
P311	Call a POISON CENTER or doctor/physician.
P312	Call a POISON CENTER or doctor/physician if you feel unwell.
P313	Get medical advice/attention.
P314	Get medical advice/attention if you feel unwell.
P315	Get immediate medical advice/attention.
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P302 + P352	IF ON SKIN: wash with plenty of soap and water.
P321
P322
P330	Rinse mouth.
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P332	IF SKIN irritation occurs:
P333	If skin irritation or rash occurs:
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P376	Stop leak if safe to do so. Oxidising gases (section 2.4) 1
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P378
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P390	Absorb spillage to prevent material damage.
P391	Collect spillage. Hazardous to the aquatic environment
P301 + P310	IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.
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P301 + P330 + P331	IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.
P302 + P334	IF ON SKIN: Immerse in cool water/wrap in wet bandages.
P302 + P350	IF ON SKIN: Gently wash with plenty of soap and water.
P303 + P361 + P353	IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P304 + P312	IF INHALED: Call a POISON CENTER or doctor/physician if you feel unwell.
P304 + P340	IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P304 + P341	IF INHALED: If breathing is difficult, remove victim to fresh air and keep at rest in a position comfortable for breathing.
P305 + P351 + P338	IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing.
P306 + P360	IF ON CLOTHING: Rinse Immediately contaminated CLOTHING and SKIN with plenty of water before removing clothes.
P307 + P311	IF exposed: call a POISON CENTER or doctor/physician.
P308 + P313	IF exposed or concerned: Get medical advice/attention.
P309 + P311	IF exposed or if you feel unwell: call a POISON CENTER or doctor/physician.
P332 + P313	IF SKIN irritation occurs: Get medical advice/attention.
P333 + P313	IF SKIN irritation or rash occurs: Get medical advice/attention.
P335 + P334	Brush off loose particles from skin. Immerse in cool water/wrap in wet bandages.
P337 + P313	IF eye irritation persists: Get medical advice/attention.
P342 + P311	IF experiencing respiratory symptoms: call a POISON CENTER or doctor/physician.
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Physical hazards
Code	Phrase
H200	Unstable explosive
H201	Explosive; mass explosion hazard
H202	Explosive; severe projection hazard
H203	Explosive; fire, blast or projection hazard
H204	Fire or projection hazard
H205	May mass explode in fire
H220	Extremely flammable gas
H221	Flammable gas
H222	Extremely flammable aerosol
H223	Flammable aerosol
H224	Extremely flammable liquid and vapour
H225	Highly flammable liquid and vapour
H226	Flammable liquid and vapour
H227	Combustible liquid
H228	Flammable solid
H229	Pressurized container: may burst if heated
H230	May react explosively even in the absence of air
H231	May react explosively even in the absence of air at elevated pressure and/or temperature
H240	Heating may cause an explosion
H241	Heating may cause a fire or explosion
H242	Heating may cause a fire
H250	Catches fire spontaneously if exposed to air
H251	Self-heating; may catch fire
H252	Self-heating in large quantities; may catch fire
H260	In contact with water releases flammable gases which may ignite spontaneously
H261	In contact with water releases flammable gas
H270	May cause or intensify fire; oxidizer
H271	May cause fire or explosion; strong oxidizer
H272	May intensify fire; oxidizer
H280	Contains gas under pressure; may explode if heated
H281	Contains refrigerated gas; may cause cryogenic burns or injury
H290	May be corrosive to metals
Health hazards
Code	Phrase
H300	Fatal if swallowed
H301	Toxic if swallowed
H302	Harmful if swallowed
H303	May be harmful if swallowed
H304	May be fatal if swallowed and enters airways
H305	May be harmful if swallowed and enters airways
H310	Fatal in contact with skin
H311	Toxic in contact with skin
H312	Harmful in contact with skin
H313	May be harmful in contact with skin
H314	Causes severe skin burns and eye damage
H315	Causes skin irritation
H316	Causes mild skin irritation
H317	May cause an allergic skin reaction
H318	Causes serious eye damage
H319	Causes serious eye irritation
H320	Causes eye irritation
H330	Fatal if inhaled
H331	Toxic if inhaled
H332	Harmful if inhaled
H333	May be harmful if inhaled
H334	May cause allergy or asthma symptoms or breathing difficulties if inhaled
H335	May cause respiratory irritation
H336	May cause drowsiness or dizziness
H340	May cause genetic defects
H341	Suspected of causing genetic defects
H350	May cause cancer
H351	Suspected of causing cancer
H360	May damage fertility or the unborn child
H361	Suspected of damaging fertility or the unborn child
H361d	Suspected of damaging the unborn child
H362	May cause harm to breast-fed children
H370	Causes damage to organs
H371	May cause damage to organs
H372	Causes damage to organs through prolonged or repeated exposure
H373	May cause damage to organs through prolonged or repeated exposure
Environmental hazards
Code	Phrase
H400	Very toxic to aquatic life
H401	Toxic to aquatic life
H402	Harmful to aquatic life
H410	Very toxic to aquatic life with long-lasting effects
H411	Toxic to aquatic life with long-lasting effects
H412	Harmful to aquatic life with long-lasting effects
H413	May cause long-lasting harmful effects to aquatic life
H420	Harms public health and the environment by destroying ozone in the upper atmosphere

[ CAS No. 937-75-7 ]

Quality Control of [ 937-75-7 ]

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[ 937-75-7 ] Synthesis Path-Downstream 1~31

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