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Chemical Structure| 94166-58-2 Chemical Structure| 94166-58-2

Structure of 94166-58-2

Chemical Structure| 94166-58-2

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Product Details of [ 94166-58-2 ]

CAS No. :94166-58-2
Formula : C7H9N3O3
M.W : 183.16
SMILES Code : O=[N+](C1=CC=C(OC)N=C1NC)[O-]
MDL No. :MFCD08741432
InChI Key :RSFNGZVULJTWHW-UHFFFAOYSA-N
Pubchem ID :3023914

Safety of [ 94166-58-2 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P264-P271-P280-P302+P352-P304+P340-P305+P351+P338-P312-P362-P403+P233-P501

Application In Synthesis of [ 94166-58-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 94166-58-2 ]

[ 94166-58-2 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 124-41-4 ]
  • [ 33742-70-0 ]
  • [ 94166-58-2 ]
  • 2
  • [ 33742-70-0 ]
  • [ 94166-58-2 ]
YieldReaction ConditionsOperation in experiment
With sodium chloride; sodium methylate; In methanol; PREPARATION 67 6-Methoxy-2-methylamino-3-nitropyridine 19 ml of a 28% methanolic solution of sodium methoxide were added dropwise to a solution of 6.00 g of <strong>[33742-70-0]6-chloro-2-methylamino-3-nitropyridine</strong> (prepared as described in Preparation 66) in 120 ml of methanol at room temperature, and the resulting mixture was stirred at room temperature for 3 hours. At the end of this time, the reaction mixture was poured into water, after which it was extracted with ethyl acetate. The extract was washed with an aqueous solution of sodium chloride and dried over anhydrous sodium sulfate, after which the solvent was removed by distillation under reduced pressure. The residue was crystallized by trituration with ethanol, to give 5.34 g of the title compound, melting at 152-153 C.
 

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