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Chemical Structure| 943982-60-3 Chemical Structure| 943982-60-3

Structure of 943982-60-3

Chemical Structure| 943982-60-3

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Product Details of [ 943982-60-3 ]

CAS No. :943982-60-3
Formula : C9H4BrCl2N3O
M.W : 320.96
SMILES Code : O=C(Cl)C1=CC(Br)=NN1C2=NC=CC=C2Cl
MDL No. :MFCD21606925

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Application In Synthesis of [ 943982-60-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 943982-60-3 ]

[ 943982-60-3 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 943982-60-3 ]
  • [ 66176-17-8 ]
  • [ 934406-08-3 ]
  • 2
  • [ 943982-60-3 ]
  • [ 66176-17-8 ]
  • [ 1233882-11-5 ]
  • 3
  • [ 943982-60-3 ]
  • [ 36764-94-0 ]
  • [ 1370337-81-7 ]
YieldReaction ConditionsOperation in experiment
With pyridine; In dichloromethane;Reflux; General procedure: A solution of 2,4,6-trisubstitutedphenylamine (10, 0.8 mmol) in pyridine (10 mL) was added to the flask containingt he crude acyl chloride 8 (0.8 mmol) which was prepared from the procedure described above, and the mixture was refluxed for 3-5 h. After cooling down, the mixture was poured into water (50 mL) and extracted with ethyl acetate (3× 15 mL). The extracts were combined and washed with hydrochloric acid (2 × 10 mL) and brine, successively. The organic phase was dried over anhydrous Na2SO4. After solvent removal, the residue was further purified by recrystallization from ethanol to afford the title compound 12(a-c) as a solid.
 

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