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Chemical Structure| 944151-83-1 Chemical Structure| 944151-83-1

Structure of 944151-83-1

Chemical Structure| 944151-83-1

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Product Details of [ 944151-83-1 ]

CAS No. :944151-83-1
Formula : C30H23N
M.W : 397.51
SMILES Code : C1(C2=CC=C(C3=CC=C(C4=CC=CC=C4)C=C3)C=C2)=CC=C(NC5=CC=CC=C5)C=C1

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Application In Synthesis of [ 944151-83-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 944151-83-1 ]

[ 944151-83-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 50548-45-3 ]
  • [ 944151-83-1 ]
  • C42H29NO [ No CAS ]
YieldReaction ConditionsOperation in experiment
82% With bis(tri-t-butylphosphine)palladium(0); sodium t-butanolate; In 5,5-dimethyl-1,3-cyclohexadiene; for 6h;Inert atmosphere; Reflux; To a 500 ml round bottom flask in a nitrogen atmosphereCompound 1-Bromobenzofuran (10.0 g, 40.65 mmol),N-phenyl- [1,1 ': 4', 1 ": 4", 1 "'-tetraphenyl] (N-phenyl- [1,1 ': 4', 1 ": 4", 1 "-quaterphenyl] -4-amine (17.75 g, 44.72 mmol) Xylene(Xylene) dissolved in 330 ml Sodium tert-butoxide(sodium tert-butoxide) (5.08 g, 52.85 mol), And bis (tri-tert-butylphosphine) palladium (0)(Bis (tri-tert-butylphosphine) palladium (0)) (0.21 g, 0.41 mmol)And the mixture was heated and stirred for 6 hours.After the temperature was lowered to room temperature and the salt was removed by filtration, xylene was concentrated under reduced pressure and recrystallized from 250 ml of ethyl acetate to obtain Compound 7 (18.89 g, yield: 82percent).
 

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