Home Cart Sign in  
Chemical Structure| 947617-22-3 Chemical Structure| 947617-22-3

Structure of 947617-22-3

Chemical Structure| 947617-22-3

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 947617-22-3 ]

CAS No. :947617-22-3
Formula : C10H10B2O4
M.W : 215.81
SMILES Code : OB(C1=C2C(B(O)O)=CC=CC2=CC=C1)O

Safety of [ 947617-22-3 ]

Application In Synthesis of [ 947617-22-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 947617-22-3 ]

[ 947617-22-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 10485-09-3 ]
  • [ 947617-22-3 ]
  • bis-2-indenyl-1,8-naphthalene [ No CAS ]
YieldReaction ConditionsOperation in experiment
33% The synthesis of the naphthyl ligand is shown in scheme 2. <strong>[10485-09-3]2-bromoindene</strong> (6.66 g, 0.0342 moles) was taken in a round-bottomed flask and dissolved in toluene. Tetrakis triphenyl phosphine palladium (0.054gm, 8mol%) was added to the above solution and stirred for 10-15 min. To this solution the diboronic acid from step 1 (3g, 0.0156 moles) dissolved in ethanol (5ml) was added, followed by aqueous sodium carbonate (2M, 10ml). The reaction mixture was heated to 80C and stirred for 24hrs. It was cooled and extracted with dichloromethane (DCM; 5 x 50ml). The DCM portion was then extracted with water (2 x 50ml), dried over sodium sulfate and concentrated. The crude compound was purified by column chromatography by continuously eluting with hexane as the eluent. Crude yield = 3g; Purified yield = 1.6g (33%)
 

Historical Records

Categories