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Chemical Structure| 952732-55-7 Chemical Structure| 952732-55-7

Structure of 952732-55-7

Chemical Structure| 952732-55-7

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Product Details of [ 952732-55-7 ]

CAS No. :952732-55-7
Formula : C7H10N2O2
M.W : 154.17
SMILES Code : O=C(C1=CNC=N1)OC(C)C

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Application In Synthesis of [ 952732-55-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 952732-55-7 ]

[ 952732-55-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1072-84-0 ]
  • [ 67-63-0 ]
  • [ 952732-55-7 ]
YieldReaction ConditionsOperation in experiment
a) lsopropyl 4-imidazolecarboxylate; To <strong>[1072-84-0]imidazole-4-carboxylic acid</strong> (CASNo. 1072-84-0, 3.0 g, 26.7 mmol) in propan-2-ol (60 mL) is added thionyl chloride (15.9 g, 13.4 mmol) and the solution is refluxed overnight. The volatiles are removed in vacuo and the residue is partitioned between ethyl acetate and 4M aqueous sodium hydroxide. The organic layer is dried over Na2SO4, filtered and concentrated to afford <strong>[1072-84-0]imidazole-4-carboxylic acid</strong> isopropyl ester; MS: (ESI) m/z 155.0 (M+H)+.
 

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