Home Cart Sign in  
Chemical Structure| 95501-85-2 Chemical Structure| 95501-85-2

Structure of 95501-85-2

Chemical Structure| 95501-85-2

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 95501-85-2 ]

CAS No. :95501-85-2
Formula : C5H12N2OS
M.W : 148.23
SMILES Code : CC(NCSCCN)=O
MDL No. :MFCD19205706

Safety of [ 95501-85-2 ]

Application In Synthesis of [ 95501-85-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 95501-85-2 ]

[ 95501-85-2 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 156-57-0 ]
  • [ 625-51-4 ]
  • [ 95501-85-2 ]
YieldReaction ConditionsOperation in experiment
Cysteamine hydrochloride (15g, 0.132mol) was dissolved in 105ml of TFA. The solution was stirred at rt for 30min and a solution of <strong>[625-51-4]acetamidomethanol</strong> (12.3g, 0.138mol) in 30ml TFA was then added. The stirring was continued for additional 2.5h. After evaporation most of the TFA, 600ml of distilled water were added. The solution was cooled by ice bath and brought to pH= 9 using concentrated NH4OH and then saturated with NaCl. The product was extracted with CHCl3/isopropanol 3:1 (6 x 300ml). The organic layer was dried over Na2SO4, evaporated to dryness and placed in vacuum desiccator overnight, yielding 8.82g (45%) of yellow oil (2). This crude substance was used without purification in the next step.
  • 2
  • [ 625-51-4 ]
  • [ 60-23-1 ]
  • [ 95501-85-2 ]
YieldReaction ConditionsOperation in experiment
In trifluoroacetic acid; at 20℃; for 3h; The mixture of cysteamine (1.15 g) and <strong>[625-51-4]acetamidemethanol</strong> (1 g) weredissolved in TF A ( triflouroacetic acid), and were stirred at room temperature for 3 hours toyield (S-acetamidomethyl) cysteamine 7 with molecular weight of 148 Da; while the found(M+H) ion peak is 149 Da.
 

Historical Records

Technical Information

Categories