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CAS No. : | 95546-96-6 | MDL No. : | MFCD01106275 |
Formula : | C11H12N2S | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 204.29 | Pubchem ID : | - |
Synonyms : |
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Signal Word: | Class: | ||
Precautionary Statements: | UN#: | ||
Hazard Statements: | Packing Group: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
96% | In ethanol for 3h; Ambient temperature; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
92% | With triethylamine In ethanol at 40 - 45℃; for 4h; | |
78% | With piperidine In ethanol for 4h; Heating; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
94% | With sodium hydroxide; iodine In ethanol for 1h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
67% | With sodium ethanolate In ethanol for 2h; Heating; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
75% | With potassium hydroxide In N,N-dimethyl-formamide at 10 - 15℃; for 0.5h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
93% | With potassium hydroxide In N,N-dimethyl-formamide at 20 - 25℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
73% | With potassium hydroxide In N,N-dimethyl-formamide at 10 - 15℃; for 0.5h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
79% | With potassium hydroxide In N,N-dimethyl-formamide at 20 - 25℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
86% | With potassium hydroxide In N,N-dimethyl-formamide at 10 - 15℃; for 0.5h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
84% | With potassium hydroxide In N,N-dimethyl-formamide at 20 - 25℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
82% | With potassium hydroxide In N,N-dimethyl-formamide at 20 - 25℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
89% | With potassium hydroxide In N,N-dimethyl-formamide at 10 - 15℃; for 0.5h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
97% | With potassium hydroxide In N,N-dimethyl-formamide at 10 - 15℃; for 0.5h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
77% | In N,N-dimethyl-formamide for 0.333333h; Heating; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: 73 percent / 10percent aq. KOH / dimethylformamide / 0.5 h / 10 - 15 °C 2: 10percent aq. KOH / dimethylformamide |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: 93 percent / 10percent aq. KOH / dimethylformamide / 20 - 25 °C 2: 82 percent / 4 h / Heating | ||
Multi-step reaction with 3 steps 1: 73 percent / 10percent aq. KOH / dimethylformamide / 0.5 h / 10 - 15 °C 2: 10percent aq. KOH / dimethylformamide 3: 82 percent / 4 h / Heating |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: 84 percent / 10percent aq. KOH / dimethylformamide / 20 - 25 °C 2: 98 percent / 0.5 h / Heating | ||
Multi-step reaction with 3 steps 1: 89 percent / 10percent aq. KOH / dimethylformamide / 0.5 h / 10 - 15 °C 2: 10percent aq. KOH / dimethylformamide 3: 98 percent / 0.5 h / Heating |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: 86 percent / 10percent aq. KOH / dimethylformamide / 0.5 h / 10 - 15 °C 2: 10percent aq. KOH / dimethylformamide |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: 89 percent / 10percent aq. KOH / dimethylformamide / 0.5 h / 10 - 15 °C 2: 10percent aq. KOH / dimethylformamide |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: 97 percent / 10percent aq. KOH / dimethylformamide / 0.5 h / 10 - 15 °C 2: 81 percent / sodium ethoxide / ethanol / 3 h / Heating |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: 77 percent / dimethylformamide / 0.33 h / Heating 2: 2.40 g / ethanol / 3 h / Heating |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: sodium ethanolate / ethanol / 20 °C 2: acetic acid / 24 h / Heating |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
84% | With acetic acid for 24h; Heating; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
94% | With sodium ethanolate In ethanol for 0.166667h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: sodium ethanolate / ethanol / 0.17 h 2: N,N-dimethyl-formamide |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In ethanol at 20℃; for 3h; regioselective reaction; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With triethylamine In ethanol at 20℃; regioselective reaction; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
68% | With potassium hydroxide In water; N,N-dimethyl-formamide at 20℃; for 26h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
75% | With sodium In ethanol at 20℃; for 26h; Reflux; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
56% | With sodium In ethanol at 20℃; for 28h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With potassium hydroxide In water; N,N-dimethyl-formamide at 15℃; Overall yield = 53 %; Overall yield = 0.4 g; |