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CAS No. : | 960067-33-8 | MDL No. : | MFCD16996403 |
Formula : | C13H17BF2O3 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | ZIBYFIJKYIKOEX-UHFFFAOYSA-N |
M.W : | 270.08 | Pubchem ID : | 53216768 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
90.2% | With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate In 1,4-dioxane at 85℃; for 16 h; Inert atmosphere | 2-Bromodifluoromethylphenylether (1 g, 4.5 mmol) and bis(pinacolato)diboron (1.71 g, 6.75 mmol) were dissolved in dioxane (10 mL), and anhydrous potassium acetate (1.1 g, 13.53 mmol) and [1,1'-bis (diphenylphosphino)ferrocene]dichloropalladium.dichloromethane (369 mg, 0.45 mmol) were added. Under nitrogen gas atmosphere, the mixture was heated to 85° C. and stirred for 16 hours. After cooling to room temperature, the reaction was concentrated under reduced pressure. The residue was purified by silica gel column chromatography (petroleum ether: ethyl acetate=10:1) to give 10-a as a pale yellow oil (1.1 g, yield 90.2percent). |
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