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Chemical Structure| 96407-89-5 Chemical Structure| 96407-89-5

Structure of 96407-89-5

Chemical Structure| 96407-89-5

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Product Details of [ 96407-89-5 ]

CAS No. :96407-89-5
Formula : C13H7BrOS
M.W : 291.16
SMILES Code : O=C1C2=C(C=C(Br)C=C2)SC3=CC=CC=C31
MDL No. :MFCD14711439
InChI Key :OFMHWHCQUXKSFK-UHFFFAOYSA-N
Pubchem ID :15593708

Safety of [ 96407-89-5 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H228
Precautionary Statements:P240-P210-P241-P280-P370+P378
Class:4.1
UN#:1325
Packing Group:

Application In Synthesis of [ 96407-89-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 96407-89-5 ]

[ 96407-89-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 870119-58-7 ]
  • [ 96407-89-5 ]
  • C31H19NOS [ No CAS ]
YieldReaction ConditionsOperation in experiment
4.8 g With potassium phosphate; tetrakis(triphenylphosphine) palladium(0); In 1,4-dioxane; at 90℃; for 4h;Inert atmosphere; In a 500mL reaction flask, add intermediate M3 (8.44g, 29mmol), M5 (10.70g, 29mmol), dioxane (100mL),K3PO4 (12.35g, 58.16mmol), Pd (PPh3) 4 (6.72g, 5.82mmol) were added, heated to 90 C under nitrogen protection, and reacted for 4 hours. The reaction was monitored by TLC, the solids were filtered off, the solution was concentrated and passed through silica gel Column purification gave a yellow solid, which was recrystallized from toluene to give 4.8 g of white compound C1.
 

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