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Chemical Structure| 96534-02-0 Chemical Structure| 96534-02-0

Structure of 96534-02-0

Chemical Structure| 96534-02-0

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Product Details of [ 96534-02-0 ]

CAS No. :96534-02-0
Formula : C13H19O5P
M.W : 286.26
SMILES Code : CCOP(=O)(CC1=CC=CC(=C1)C(=O)OC)OCC
MDL No. :MFCD18800849

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Application In Synthesis of [ 96534-02-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 96534-02-0 ]

[ 96534-02-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 54439-75-7 ]
  • [ 96534-02-0 ]
  • C17H15ClO3 [ No CAS ]
YieldReaction ConditionsOperation in experiment
51% To a solution of compound B6 (14.3 g, 50 mmol) in 70 ml_ of dry THF was added sodium hydride (2.4 g, 60 mmol) at 0°C for 30 mins. To this resulting mixture was added the solution of compound E2 (8.5 g, 50 mmol) in 50 ml_ of dry THF at 0°C, and the solution was stirred at room temperature for 3 h. The mixture was quenched by sat. NH4CI solution and extracted with EtOAc. The organic layer was washed with brine, dried over Na2SO4, filtered, concentrated and purified by flash chromatography on silica gel (eluent: PE/EA = 50/1) to give 7.7 g of compound N1 as a white solid (Yield: 51percent).
 

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