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Chemical Structure| 96604-27-2 Chemical Structure| 96604-27-2

Structure of 96604-27-2

Chemical Structure| 96604-27-2

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Product Details of [ 96604-27-2 ]

CAS No. :96604-27-2
Formula : C11H11Cl2NO
M.W : 244.12
SMILES Code : CN(C(/C=C/C1=CC(Cl)=CC(Cl)=C1)=O)C
MDL No. :MFCD04967390

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Application In Synthesis of [ 96604-27-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 96604-27-2 ]

[ 96604-27-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 14401-72-0 ]
  • [ 4637-24-5 ]
  • [ 96604-27-2 ]
YieldReaction ConditionsOperation in experiment
12.3 g for 3h;Reflux; 3?,S?-Dichloroacetophenone (9.7 g, 51 mmol) was heated at reflux in N,N-dimethylformamide dimethylacetal (50 mL) for 3 h. After cooling to ambient temperature, the reaction mixture was concentrated and dried under vacuum to give of anorange solid (12.3 g) that was used without further purification.1HNMRoe 7.82 (d, 1H), 7.74 (s, 2H), 7.42 (s, 1H), 5.58 (d, 1H), 3.18 (bs, 3H), 2.95 (bs, 3H).
 

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