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Chemical Structure| 97267-35-1 Chemical Structure| 97267-35-1

Structure of 97267-35-1

Chemical Structure| 97267-35-1

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Product Details of [ 97267-35-1 ]

CAS No. :97267-35-1
Formula : C13H17NO
M.W : 203.28
SMILES Code : N(CCC1)(CC2=CC=CC=C2)CC31CO3

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Application In Synthesis of [ 97267-35-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 97267-35-1 ]

[ 97267-35-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1774-47-6 ]
  • [ 50606-58-1 ]
  • [ 97267-35-1 ]
YieldReaction ConditionsOperation in experiment
With potassium hydroxide; In acetonitrile; at 50℃; for 2.5h; Ground 85% potassium hydroxide (5.2 g) was added to a suspension of <strong>[50606-58-1]1-benzyl-3-piperidone hydrochloride</strong> hydrate (5.0 g) and trimethylsulfoxonium iodide (5.3 g) in anhydrous acetonitrile (220 mL), followed by stirring at 50C under nitrogen atmosphere for two and half hours. After cooling to room temperature, insoluble matter was removed by filtration, and the filtrate was concentrated under reduced pressure. The residue was mixed with ethyl acetate (100 mL) and water (50 mL) and was separated. The organic layer was sequentially washed with water (50 mL) and brine (50 mL) and was dried over anhydrous sodium sulfate. The solvent was removed under reduced pressure to yield the titled compound (4.07 g) as an oil.
 

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