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Chemical Structure| 626-29-9 Chemical Structure| 626-29-9
Chemical Structure| 626-29-9

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Product Details of Myristic anhydride

CAS No. :626-29-9
Formula : C28H54O3
M.W : 438.73
SMILES Code : CCCCCCCCCCCCCC(OC(CCCCCCCCCCCCC)=O)=O
English Name :MYristic anhydride
MDL No. :MFCD00056151
InChI Key :RCRYHUPTBJZEQS-UHFFFAOYSA-N
Pubchem ID :69377

Safety of Myristic anhydride

Application In Synthesis of Myristic anhydride

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 626-29-9 ]

[ 626-29-9 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 56-81-5 ]
  • [ 626-29-9 ]
  • [ 589-68-4 ]
YieldReaction ConditionsOperation in experiment
13 % Chromat. With Candida antarctica In 1,4-dioxane at 15℃; for 4h;
  • 2
  • [ 98796-51-1 ]
  • [ 626-29-9 ]
  • [ CAS Unavailable ]
YieldReaction ConditionsOperation in experiment
82.2% With N-ethyl-N,N-diisopropylamine In tetrahydrofuran at 20℃; for 72h; Inert atmosphere; Further stages; 30 Example 30: Synthesis of 5’-O-DMTr-dCMyr-dCMyr-dCMyr-dCMyr-dT-suc-NH-TPB General procedure: Under an argon atmosphere, 5'-O-(4,4'-dimethoxytrityl)-2'-deoxycytidine-3'-O-[(2-cyanoethyl)-N,N-diisopropylphosphoramidite] (20.4 g, 28.0 mmol) was dissolved in tetrahydrofuran (200 ml), N,N-diisopropylethylamine (7.4 g, 57.0 mmol) and 2-ethyl-1-hexanoic anhydride (11.4 g, 42.0 mmol) were added, and the mixture was stirred at room temperature for 3 days. To the reaction mixture after completion of the reaction were added ethyl acetate and water, and the mixture was extracted. The ethyl acetate layer was washed with 5% aqueous sodium hydrogen carbonate solution and saturated brine. The organic layer was dried over anhydrous sodium sulfate, the solvent was evaporated under reduced pressure, and the obtained crude product was purified by silica gel column chromatography (eluate; 1% triethylamine-containing 10:1→1:1 heptane-ethyl acetate) to give the title compound (15.9 g, 66.5%).0420] Based on the method described in Example 27, the title compound (199 mg, 82.2%) was obtained from 5’-ODMTr-dT-suc-NH-TPB (102 mg, 63.1 mmol) by repeating elongation of cytidine derivative 4 times using the phosphoramiditemonomer described in Example 24.thin layer chromatography: Rf 0.14 (eluent = ethyl acetate)
  • 3
  • [ 13734-41-3 ]
  • [ 13139-15-6 ]
  • [ 15761-38-3 ]
  • [ 30992-29-1 ]
  • [ 15260-10-3 ]
  • [ 13836-37-8 ]
  • C100H145ClN19O23PolS [ No CAS ]
  • [ 73821-95-1 ]
  • [ 18942-49-9 ]
  • [ 73821-97-3 ]
  • [ 6404-28-0 ]
  • [ 55260-24-7 ]
  • [ 25024-53-7 ]
  • [ 626-29-9 ]
  • cyclo(30−33)[D-Phe12, Nle21,38,Aib27,32,40,Glu30,Lys33]-tetradecanoyl-{human/rat corticotropin releasing factor}(9−41) [ No CAS ]
 

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