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Chemical Structure| 10027-80-2 Chemical Structure| 10027-80-2

Structure of 10027-80-2

Chemical Structure| 10027-80-2

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Product Details of [ 10027-80-2 ]

CAS No. :10027-80-2
Formula : C6H16Cl2N2
M.W : 187.11
SMILES Code : N[C@H]1[C@@H](N)CCCC1.[H]Cl.[H]Cl
MDL No. :MFCD19440709

Safety of [ 10027-80-2 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338

Application In Synthesis of [ 10027-80-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 10027-80-2 ]

[ 10027-80-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 10027-80-2 ]
  • [ 100-52-7 ]
  • [ 65838-10-0 ]
YieldReaction ConditionsOperation in experiment
77% With dirhodium tetraacetate; carbon monoxide; In water; isopropyl alcohol; at 140℃; under 3800.26 - 38002.6 Torr; for 4h;Autoclave; General procedure: A glass vial in a 10 mL stainless steel autoclave was charged with Rh2(OAc)4 (0.7 mg, 1.60 mumol, 1mol%), (R,R)-1,2-cyclohexanediammonium chloride (30.0 mg, 0.160 mmol, 100 mol%),isopropanol (0.1 mL), water (0.1 mL) and aldehyde (0.320 mmol, 200 mol%). The autoclave wassealed, flushed three times with 5 atm of CO, and then charged with 50 atm of CO. The reactor wasplaced into a preheated oil bath (140 C). After 4 h, the reactor was cooled to room temperature anddepressurized. The residue was filtrated from precipitate and analyzed by 1H NMR.
 

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