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[ CAS No. 1026-05-7 ]

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Chemical Structure| 1026-05-7
Chemical Structure| 1026-05-7
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CAS No. :1026-05-7 MDL No. :MFCD00183927
Formula : C16H18N2 Boiling Point : 400.4±44.0°C at 760 mmHg
Linear Structure Formula :- InChI Key :-
M.W :238.33 g/mol Pubchem ID :2839906
Synonyms :

Safety of [ 1026-05-7 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P280-P305+P351+P338 UN#:N/A
Hazard Statements:H302 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 1026-05-7 ]

  • Upstream synthesis route of [ 1026-05-7 ]
  • Downstream synthetic route of [ 1026-05-7 ]

[ 1026-05-7 ] Synthesis Path-Upstream   1~8

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YieldReaction ConditionsOperation in experiment
82% With DPZ In chloroform; toluene at 25℃; for 15 h; Molecular sieve; Sealed tube; Irradiation; Green chemistry Will dissolve in 200μLOrganic photocatalyst DPZ in toluene (0.28 mg, 0.0008 mmol)Take a 10mL reaction flask,Dry the toluene with an air pump and add 66 mg (0.4 mmol)2-phenylaminopropionic acid and 100mg 4Å molecular sieves,Then add 4mL purified and dried chloroform and seal the bottle mouth with a rubber stopper.And insert a balloon filled with dry air. Place the reaction flask in a 25°C incubator.The reaction was stirred for 15 hours under the irradiation of two 1W blue LED lamps.After the reaction is complete, use a rotary evaporator to distill 2/3 of the solution.Separation by column chromatography (hexane/ethyl acetate 60-30:1)That is, 39.1 mg of 2-methyl-4-N-phenyl-tetrahydroquinolin-4-amine are obtained as a colorless oily liquid.The yield was 82percent.
Reference: [1] Patent: CN108017579, 2018, A, . Location in patent: Paragraph 0008; 0011; 0012
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  • [ 75-07-0 ]
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Reference: [1] Patent: WO2004/72041, 2004, A1, . Location in patent: Page/Page column 79-80
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  • [ 2028-84-4 ]
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Reference: [1] Tetrahedron Letters, 1990, vol. 31, # 14, p. 2069 - 2072
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  • [ 112825-69-1 ]
Reference: [1] Tetrahedron Letters, 1990, vol. 31, # 14, p. 2069 - 2072
  • 5
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  • [ 3684-12-6 ]
  • [ 27356-66-7 ]
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Reference: [1] Advanced Synthesis and Catalysis, 2018, vol. 360, # 9, p. 1754 - 1760
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Reference: [1] Tetrahedron Letters, 1990, vol. 31, # 14, p. 2069 - 2072
[2] Tetrahedron Letters, 1990, vol. 31, # 14, p. 2069 - 2072
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  • [ 64-17-5 ]
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  • [ 32142-34-0 ]
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Reference: [1] Synthesis and Reactivity in Inorganic, Metal-Organic and Nano-Metal Chemistry, 2013, vol. 43, # 4, p. 500 - 508
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Reference: [1] Bulletin of the Chemical Society of Japan, 1969, vol. 42, p. 2885
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