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Chemical Structure| 102791-87-7 Chemical Structure| 102791-87-7

Structure of 102791-87-7

Chemical Structure| 102791-87-7

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Product Details of [ 102791-87-7 ]

CAS No. :102791-87-7
Formula : C10H11N3
M.W : 173.21
SMILES Code : CC1=CN(C=N1)C1=CC=C(N)C=C1
MDL No. :MFCD09834629
InChI Key :PJUPTRYCQKQLCI-UHFFFAOYSA-N
Pubchem ID :16005170

Safety of [ 102791-87-7 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 102791-87-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 102791-87-7 ]

[ 102791-87-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 102791-87-7 ]
  • [ 17823-69-7 ]
  • [ 1456732-83-4 ]
YieldReaction ConditionsOperation in experiment
Dissolved 0.500 g <strong>[17823-69-7]2-cyano-3,3-bis(methylthio)acrylamide</strong> in 15 mL EtOH and added 4-methyl-l-(4-aminophenyl)-lH-imidazole (1.0 eq.) . Stirred reaction at 75 C until starting amide was absent by HPLC. Once complete (18 hrs), reaction was brought to room temperature and filtered to obtain a light yellow powder as product. Product was allowed to dry under vacuum for 1 hr. Product was then suspended in 10 mL EtOH and hydrazine hydrate (1 eq.) was added dropwise. Reaction was heated at 75 C until intermediate was absent (HPLC). Once intermediate was absent (18 hrs), reaction was brought to room temperature and filtered to obtain 5 -amino-3-((4-(4-methyl-l H-imidazol- 1 -yl)phenyl)amino)- lH-pyrazole-4-carboxamide as a yellow powder. Product was allowed to dry under vacuum for 1 hr. H3C 5-amino-3-((4-(4-methyl-lH-imidazol-l-yl)phenyl)amino)-lH-pyrazole-4-carboxamide
 

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