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[ CAS No. 10289-45-9 ]

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2D
Chemical Structure| 10289-45-9
Chemical Structure| 10289-45-9
Structure of 10289-45-9 *Storage: {[proInfo.prStorage]}

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Product Details of [ 10289-45-9 ]

CAS No. :10289-45-9MDL No. :MFCD00102114
Formula : C15H16 Boiling Point : 304.4°C at 760 mmHg
Linear Structure Formula :-InChI Key :-
M.W :196.29Pubchem ID :2734126
Synonyms :

Computed Properties of [ 10289-45-9 ]

TPSA : 0 H-Bond Acceptor Count : 0
XLogP3 : - H-Bond Donor Count : 0
SP3 : 0.20 Rotatable Bond Count : 3

Safety of [ 10289-45-9 ]

Signal Word:WarningClass:N/A
Precautionary Statements:P261-P305+P351+P338UN#:N/A
Hazard Statements:H302-H315-H319-H335Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 10289-45-9 ]

  • Upstream synthesis route of [ 10289-45-9 ]
  • Downstream synthetic route of [ 10289-45-9 ]

[ 10289-45-9 ] Synthesis Path-Upstream   1~2

  • 1
  • [ 10289-45-9 ]
  • [ 58743-81-0 ]
YieldReaction ConditionsOperation in experiment
77% With iron(III) chloride; bromine In dichloromethane at 25℃; for 18 h; Add 1 equivalent of compound 5, fifth organic solvent, 0.2 equivalent of ferric chloride to the reaction flask, and the fifth organic solvent is dichloromethane.The weight ratio of the fifth organic solvent to the compound 5 is 5:1, and the mixture is stirred well, and 1.15 equivalents of liquid bromine is slowly added thereto, and the temperature is maintained at 25 ° C for 18 hours.The reaction was quenched by adding a 15percent aqueous solution of sodium hydroxide, stirred, and allowed to stand for separation. The organic phase was washed twice with water to remove the aqueous phase.The organic phase was dried to give a crude compound (yield: Compound 6), which was beaten in methanol, filtered, and dried to give a white solid as compound 6 in a yield of 77percent.
Reference: [1] Patent: CN108129258, 2018, A, . Location in patent: Paragraph 0020; 0030; 0031; 0038; 0039; 0040; 0041; 0042
  • 2
  • [ 10289-45-9 ]
  • [ 58743-76-3 ]
Reference: [1] Journal of Organic Chemistry USSR (English Translation), 1984, vol. 20, p. 1187 - 1191[2] Zhurnal Organicheskoi Khimii, 1984, vol. 20, # 6, p. 1305 - 1310
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