Home Cart Sign in  
Chemical Structure| 10466-37-2 Chemical Structure| 10466-37-2

Structure of 10466-37-2

Chemical Structure| 10466-37-2

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 10466-37-2 ]

CAS No. :10466-37-2
Formula : C15H10N2
M.W : 218.25
SMILES Code : N#CC1=CC=C(CC2=CC=C(C=C2)C#N)C=C1
MDL No. :MFCD09032983
InChI Key :QHPFUQAZWHBITN-UHFFFAOYSA-N
Pubchem ID :300442

Safety of [ 10466-37-2 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338

Application In Synthesis of [ 10466-37-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 10466-37-2 ]

[ 10466-37-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 10466-37-2 ]
  • [ 79802-71-4 ]
YieldReaction ConditionsOperation in experiment
96% With potassium phosphate; 18-crown-6 ether; copper diacetate; In N,N-dimethyl acetamide; at 120℃; for 12h;Inert atmosphere; Schlenk technique; Sealed tube; In a dry Schlenck tube, add bis(4-cyanophenyl)methane (65 mg, 0.3 mmol), anhydrous copper acetate (136 mg, 0.75 mmol), potassium phosphate (150 mg, 0.75 mmol) and 18-crown-6 (16mg, 0.06mmol), then anhydrous N,N-dimethylacetamide (5 mL) was added under nitrogen atmosphere and the tube was sealed and heated for 12 hours. After the reaction mixture was cooled, 50 mL dilute hydrochloric acid (3 M) was added, the aqueous phase was extracted three times with ethyl acetate (50 mL), and the organic phases were combined and washed with saturated sodium carbonate and saturated brine each time. The organic phase was dried over anhydrous sodium sulfate, filtered, and the solvent was removed in vacuo, and then separated by silica gel chromatography column chromatography to obtain 62 mg of tetrakis(4-cyanophenyl)ethylene with a yield of 96%.
 

Historical Records

Technical Information

Categories

Related Functional Groups of
[ 10466-37-2 ]

Aryls

Chemical Structure| 46833-85-6

A310025 [46833-85-6]

3,3'-Methylenedibenzonitrile

Similarity: 1.00

Chemical Structure| 23450-31-9

A132153 [23450-31-9]

4-Benzylbenzonitrile

Similarity: 1.00

Chemical Structure| 93717-55-6

A982727 [93717-55-6]

3-Benzylbenzonitrile

Similarity: 1.00

Chemical Structure| 25309-65-3

A265120 [25309-65-3]

4-Ethylbenzonitrile

Similarity: 0.95

Chemical Structure| 34136-57-7

A134473 [34136-57-7]

3-Ethylbenzonitrile

Similarity: 0.95

Nitriles

Chemical Structure| 46833-85-6

A310025 [46833-85-6]

3,3'-Methylenedibenzonitrile

Similarity: 1.00

Chemical Structure| 23450-31-9

A132153 [23450-31-9]

4-Benzylbenzonitrile

Similarity: 1.00

Chemical Structure| 93717-55-6

A982727 [93717-55-6]

3-Benzylbenzonitrile

Similarity: 1.00

Chemical Structure| 25309-65-3

A265120 [25309-65-3]

4-Ethylbenzonitrile

Similarity: 0.95

Chemical Structure| 34136-57-7

A134473 [34136-57-7]

3-Ethylbenzonitrile

Similarity: 0.95