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[ CAS No. 10511-51-0 ] {[proInfo.proName]}

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Chemical Structure| 10511-51-0
Chemical Structure| 10511-51-0
Structure of 10511-51-0 * Storage: {[proInfo.prStorage]}
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Product Details of [ 10511-51-0 ]

CAS No. :10511-51-0 MDL No. :MFCD00022894
Formula : C16H13NO Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 235.28 Pubchem ID :-
Synonyms :

Safety of [ 10511-51-0 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P280-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H317-H319 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 10511-51-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 10511-51-0 ]
  • Downstream synthetic route of [ 10511-51-0 ]

[ 10511-51-0 ] Synthesis Path-Upstream   1~2

  • 1
  • [ 10511-51-0 ]
  • [ 27018-76-4 ]
Reference: [1] Journal of the Chilean Chemical Society, 2011, vol. 56, # 4, p. 866 - 869
[2] Archiv der Pharmazie, 1984, vol. 317, # 10, p. 847 - 851
  • 2
  • [ 54655-07-1 ]
  • [ 10511-51-0 ]
  • [ 2975-46-4 ]
YieldReaction ConditionsOperation in experiment
87% at 0℃; for 8 h; General procedure: To the ice-cold solution of aldehyde in THF was added, the solution of alkylmagnesium halide or alkyllithium in THF (1.3 eq., at 0 °C). The reaction was stirred at 0 °C for 1 h, diluted with saturated aq. NH4Cl (10 mL) and ethyl acetate (10 mL). Aqueous layer was extracted with ethyl acetate (2×10 mL). The combined organic layers were washed with brine (10 mL), and dried over Na2SO4. Evaporation of the solvent and purification of the crude mixture by column chromatography (9:1, hexane: EtOAc) gave the corresponding bisindolylmethane derivatives (BIM) up to 92percent yields along with the by-product aldehyde.
Reference: [1] Tetrahedron, 2016, vol. 72, # 49, p. 8106 - 8116
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