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Chemical Structure| 106-69-4 Chemical Structure| 106-69-4

Structure of 106-69-4

Chemical Structure| 106-69-4

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Product Details of [ 106-69-4 ]

CAS No. :106-69-4
Formula : C6H14O3
M.W : 134.17
SMILES Code : OCC(O)CCCCO
MDL No. :MFCD00002976

Safety of [ 106-69-4 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P264-P271-P280-P302+P352-P304+P340-P305+P351+P338-P312-P362-P403+P233-P501

Application In Synthesis of [ 106-69-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 106-69-4 ]

[ 106-69-4 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 51792-34-8 ]
  • [ 106-69-4 ]
  • 4-(2,3-dihydrothieno[3,4-b][1,4]dioxin-2-yl)butan-1-ol [ No CAS ]
YieldReaction ConditionsOperation in experiment
51% With toluene-4-sulfonic acid; In toluene; at 110℃; for 36h; 2.5 g of <strong>[51792-34-8]2,3-dimethoxythiophene</strong> (17.3mmol) was dissolved in toluene(100 mL). 4.6 g of hexan-1,2,6-triol (34.6 mmol) and 665 mg of paratoluenesulfonicacid monohydrate (3.5 mmol) were then added. Themixture was warmed at 110 °C for over 36 h. The mixture was thencooled at room temperature. The mixture was extracted with 5percentNaHCO3 in water (2 × 30 mL) and brine (30 mL), dried over Na2SO4.The solvents were removed under reduced pressure. EDOT-OH wasfinally purified on column (80/20, cyclohexane/ethyl acetate).Yield: 1.9 g of slightly yellow oil (51percent). Rf: 0.5 (5/5, cyclohexane/ethylacetate). 1H NMR (CDCl3): delta = 1.52?1.69 (m, 6H), 3.64?3.71(m, 2H), 3.85?3.91 (m, 1H), 4.1?4.18 (m, 2H), and 6.3 (s, 2H);13C NMR (CDCl3): delta = 21.3, 30.4, 32.4, 62.6, 68.4, 73.6, 99.3, 141.6, and142. MS: 213.9.
  • 2
  • [ 51792-34-8 ]
  • [ 106-69-4 ]
  • 2-(4-azidobutyl)-2,3-dihydrothieno[3,4-b][1,4]dioxine [ No CAS ]
 

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