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Chemical Structure| 1065102-79-5 Chemical Structure| 1065102-79-5

Structure of 1065102-79-5

Chemical Structure| 1065102-79-5

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Product Details of [ 1065102-79-5 ]

CAS No. :1065102-79-5
Formula : C8H8INO2
M.W : 277.06
SMILES Code : O=C(OC)C1=CC(N)=CC=C1I
MDL No. :MFCD17276521
InChI Key :MZYYAXWPUHHYDZ-UHFFFAOYSA-N
Pubchem ID :63022459

Safety of [ 1065102-79-5 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338

Application In Synthesis of [ 1065102-79-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1065102-79-5 ]

[ 1065102-79-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 14316-61-1 ]
  • [ 1065102-79-5 ]
  • methyl N-phenoxyacetyl-3-amino-6-iodobenzoate [ No CAS ]
YieldReaction ConditionsOperation in experiment
82.3% In N,N-dimethyl-formamide; at 0 - 20℃;Inert atmosphere; Phenoxyacetyl anhydride (2.45 g, 8.56 mmol) was added to a solution of compound 7 (1.98 g, 7.15 mmol) in DMF (15 mL) under Ar gas at 0 C. After stirring under Ar gas at room temperature for 120 min, the reaction mixture was evaporated to dryness. The crude product was purified by silica gel column chromatography (ethyl acetate:hexane 1:9 to 4:6 v/v) to obtain the desired product 8 as a light brown solid (2.42 g, 82.3%)
 

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