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[ CAS No. 1070879-30-9 ] {[proInfo.proName]}

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3d Animation Molecule Structure of 1070879-30-9
Chemical Structure| 1070879-30-9
Chemical Structure| 1070879-30-9
Structure of 1070879-30-9 * Storage: {[proInfo.prStorage]}
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Product Details of [ 1070879-30-9 ]

CAS No. :1070879-30-9 MDL No. :MFCD11505112
Formula : C9H5BrClN Boiling Point : -
Linear Structure Formula :- InChI Key :FEBLUGZKVJAOLT-UHFFFAOYSA-N
M.W : 242.50 Pubchem ID :21568282
Synonyms :

Safety of [ 1070879-30-9 ]

Signal Word:Danger Class:8,6.1
Precautionary Statements:P280-P301+P310-P305+P351+P338 UN#:2923
Hazard Statements:H301-H318 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 1070879-30-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1070879-30-9 ]

[ 1070879-30-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 4203-18-3 ]
  • [ 1070879-30-9 ]
YieldReaction ConditionsOperation in experiment
67% With trimethylsilyl bromide; propiononitrile at 100℃; for 16h; Sealed tube; 217.A Part A: 4-bromo-6-chloroquinoline To a 20 mL microwave tube was added 4,7-dichloroquinoline (0.3315 g, 1.674 mmol) and propionitrile (3 mL), followed by TMS-Br (0.434 ml, 3.35 mmol) at room temperature. A precipitate was formed. The tube was sealed and heated to 100 °C for 16 h. The reaction mixture was cooled to room temperature then poured into ice-cooled NaOH (IN, 3 mL) and the tube was rinsed with water. The aqueous layer was extracted with diethyl ether (3x5 mL). The diethyl ether layers were combined, dried (Na2S04), filtered and concentrated to give the crude product as a yellow solid. The material was purified by silica gel chromatography (EtOAc in hexanes to afford 4-bromo-6-chloroquinoline (300 mg, 1.126 mmol, 67% yield) as a plae yellow solid. NMR (400MHz, CHLOROFORM-d) δ 8.70 (d, J=4.6 Hz, IH), 8.17 (d, J=8.8 Hz, IH), 8.14 (d, J=2.0 Hz, IH), 7.73 (d, J=4.6 Hz, IH), 7.63 (dd, J=9.0, 2.0 Hz, IH).
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