Home Cart Sign in  
Chemical Structure| 111205-01-7 Chemical Structure| 111205-01-7

Structure of 111205-01-7

Chemical Structure| 111205-01-7

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 111205-01-7 ]

CAS No. :111205-01-7
Formula : C10H9N3O2
M.W : 203.20
SMILES Code : O=C(OC)C1=CN=C(N2C=CN=C2)C=C1
MDL No. :MFCD00140820

Safety of [ 111205-01-7 ]

Application In Synthesis of [ 111205-01-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 111205-01-7 ]

[ 111205-01-7 ] Synthesis Path-Upstream   1~1

  • 1
  • [ 111205-01-7 ]
  • [ 216955-75-8 ]
YieldReaction ConditionsOperation in experiment
68% With sodium hydroxide In tetrahydrofuran; methanol at 50℃; for 3 h; Preparation 38Synthesis of 6-imidazol-l-ylpyridine-3-carboxylic acid.Place methyl 6-imidazol-l-ylpyridine-3-carboxylate (535 mg, 2.50 mmoles), tetrahydrofuran (12 mL), sodium hydroxide (780 mg, 3.75 mmoles) and methanol (10 mL) in a round bottom flask and heat at 50 °C for 3 hours. Acidify the reaction mixture with 1 N hydrochloric acid and concentrate under reduced pressure until dry. Suspend in methanol/dichloromethane, filter and concentrate to give the title compound as a white solid (0.47 g, 68percent). LCMS (m/z): 190.0 (M+1).
References: [1] Patent: WO2014/168824, 2014, A1, . Location in patent: Page/Page column 39; 40.
[2] Patent: WO2011/94890, 2011, A1, . Location in patent: Page/Page column 130.
 

Historical Records

Technical Information

Categories