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Type HazMat fee for 500 gram (Estimated)
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Chemical Structure| 112-13-0 Chemical Structure| 112-13-0
Chemical Structure| 112-13-0

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Synonyms: Decanoic acid chloride

4.5 *For Research Use Only !

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Product Details of Decanoyl Chloride

CAS No. :112-13-0
Formula : C10H19ClO
M.W : 190.71
SMILES Code : CCCCCCCCCC(Cl)=O
Synonyms :
Decanoic acid chloride
MDL No. :MFCD00000771
InChI Key :IPIVAXLHTVNRBS-UHFFFAOYSA-N
Pubchem ID :66982

Safety of Decanoyl Chloride

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H314
Precautionary Statements:P280-P305+P351+P338-P310
Class:8
UN#:3265
Packing Group:

Application In Synthesis of Decanoyl Chloride

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 112-13-0 ]

[ 112-13-0 ] Synthesis Path-Downstream   1~13

  • 1
  • [ 20876-36-2 ]
  • [ 112-13-0 ]
  • [ 107923-75-1 ]
  • 2
  • [ 10212-25-6 ]
  • [ 112-13-0 ]
  • [ 62840-05-5 ]
  • 4
  • [ 136-77-6 ]
  • [ 112-13-0 ]
  • [ 393519-45-4 ]
  • 6
  • [ 69-74-9 ]
  • [ 112-13-0 ]
  • [ 58611-44-2 ]
  • 7
  • [ 22876-16-0 ]
  • [ 112-13-0 ]
  • C18H25NO3 [ No CAS ]
  • 8
  • [ 7768-28-7 ]
  • [ 112-13-0 ]
  • [ 491845-56-8 ]
  • 9
  • [ 7768-28-7 ]
  • [ 112-13-0 ]
  • [ 1390634-24-8 ]
  • 10
  • [ 103755-58-4 ]
  • [ 112-13-0 ]
  • [ 1578190-83-6 ]
YieldReaction ConditionsOperation in experiment
With pyridine; dmap; In dichloromethane; at 20℃; General procedure: Into a round-bottom flask were added 5.71mmolof alditolyl-triazole 12 or 21a in 50ml dichloromethane, 0.9mL of pyridine (2 eq.), 5.71mmolof acyl chloride and catalytic amount of DMAP. The mixture was stirred vigorously at room temperature, and the reaction progress was monitored by thin layer chromatography. Next, the mixture was washed with distilled water (3×100mL), saturated sodium bicarbonate solution (5×100mL), dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure. The product was purified via silica-gel column chromatography using gradient mixture of hexane-ethyl acetate, to afford the pure derivatives 13a-k and 22a-d.
  • 11
  • [ 1221973-02-9 ]
  • [ 112-13-0 ]
  • 2,6-bis(1-decanoyl-[4S,5S]-4,5-diphenyl-4,5-dihydro-1H-imidazol-2-yl)pyridine [ No CAS ]
  • 12
  • [ 98-55-5 ]
  • [ 112-13-0 ]
  • C20H36O2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
30.83 g In tetrahydrofuran; for 3h; 34.4 g (0.2 mol) of decanoic acid, 17.85 g (0.15 mol) of thionyl chloride was added, Mixed hook at 60 C for 3 hours, 20 ml of a tetrahydrofuran solution containing 15.4 g (0 lmo 1) alpha-<strong>[98-55-5]terpineol</strong> was added, Continue to react for 3 hours, The reaction solution was adjusted to pH 6-7 with NaOH solution. The organic layer was separated and the aqueous layer was extracted with ethyl acetate. The organic layers were combined, washed with saturated brine and dried over Na2S04 overnight. The solvent was evaporated and the column chromatography For 200 to 300 mesh), B petroleum ether and ethyl acetate (15: 1) as the eluent, and the eluent was distilled off to give 30.83 g of a colorless liquid, The yield was 93.5%.
  • 13
  • [ 112-13-0 ]
  • [ 180683-64-1 ]
  • C21H40N2O3 [ No CAS ]
 

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