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CAS No. : | 67342-99-8 | MDL No. : | MFCD20127688 |
Formula : | C14H26O3 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | GUIDAPPCHUNALD-UHFFFAOYSA-N |
M.W : | 242.35 | Pubchem ID : | 3017756 |
Synonyms : |
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Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
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* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
72% | With water; sodium hydroxide; In ethanol; at 20℃; for 12h; | Compound 12-1 (647 mg, 2.67 mmol, 1 eq.) was dissolved in EtOH/H20 (10/10 mE), then added NaOH (139 mg, 3.47 mmol, 1.3 eq.). The reaction was stirred at 20 C. for 12 h. The reaction mixture was washed twice with ethyl acetate (10 mE). The aqueous layer was adjusted to acidic (pH 3-5) with iN HC1. A white solid was precipitated, filtered and dried in vacuo to obtain compound 13-1 (white solid, 410 mg, 72%). ?H NMR (300 MHz, DMSO) oe 12.53 (s, 1H), 3.43 (s, 2H), 2.39 (t, J=7.2 Hz, 2H), 1.23 (m, 14H), 0.85 (t, J=6.3 Hz, 3H). |