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Chemical Structure| 112629-69-3 Chemical Structure| 112629-69-3

Structure of 112629-69-3

Chemical Structure| 112629-69-3

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Product Details of [ 112629-69-3 ]

CAS No. :112629-69-3
Formula : C10H10N2S
M.W : 190.26
SMILES Code : N#CC1=CC2=C(NC1=S)CCCC2
MDL No. :MFCD00487216

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Application In Synthesis of [ 112629-69-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 112629-69-3 ]

[ 112629-69-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 25625-57-4 ]
  • [ 112629-69-3 ]
  • 3-amino-N-(3′-(trifluoromethyl)phenyl)-5,6,7,8-tetrahydrothieno[2,3-b]quinoline-2-carboxamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
22% With sodium carbonate; In ethanol; at 100℃; for 18h;Inert atmosphere; General procedure: A mixture of 2-bromoacetamides 12a-v (1 equiv), carbonitrile10a-c (1 equiv) and anhydrous sodium carbonate (1.06 equiv) in absolute ethanol or methanol was stirred at reflux for 18 h. The mixture was cooled to room temperature and the solvent removed in vacuo to give the crude product which was washed with small amounts of ice water before being recrystallized from methanol to give the thieno[2,3-b]pyridine-2-carboxamides 5-7.
 

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