Home Cart Sign in  
Chemical Structure| 1160573-64-7 Chemical Structure| 1160573-64-7

Structure of 1160573-64-7

Chemical Structure| 1160573-64-7

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

DE Stock

US Stock

Asia Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 1160573-64-7 ]

CAS No. :1160573-64-7
Formula : C6H2BrCl2F
M.W : 243.89
SMILES Code : FC1=C(Cl)C=C(Cl)C=C1Br
MDL No. :MFCD11845990
InChI Key :MIEOCLLZJPCOIV-UHFFFAOYSA-N
Pubchem ID :50997897

Safety of [ 1160573-64-7 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338

Application In Synthesis of [ 1160573-64-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1160573-64-7 ]

[ 1160573-64-7 ] Synthesis Path-Downstream   1~7

  • 1
  • [ 1160573-64-7 ]
  • [ 357274-85-2 ]
  • [ 1364674-30-5 ]
YieldReaction ConditionsOperation in experiment
With potassium carbonate;bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; water; for 3.0h;Inert atmosphere; Reflux; l-bromo-3,5-dichloro-2-fluorobenzene (10 g), (3,3,3-trifluoroprop-l-en-2-yl)-boronic acid (7.5 g:) and potassium carbonate (13.6 g) were dissolved in tetrahydrofuran (41 ml) and water (20 ml), and then deaerated. Dichlorobis(triphenylphosphine)palladium (II) ( 1.4 g) was added thereto and the mixture was stirred for 3 hours under reflux under argon atomosphere. After cooling the mixture to the room temperature, water and n-hexane were added, and the organic layer was washed with water and dried over anhydrous magnesium sulfate. The drying agent was filtered off, the solvent was distilled off under reduced pressure, and the residue was roughtly purified by silica gel chromatography (n-hexane) to obtain a mixture containing l,3-dichloro-2,4-difluoro-5-(3,3,3-trifluoroprop-l-en-2-yl)benzene and hexane. i-NMR (CDC13) δ: 5.82 (1H, s), 6.25 (1H, s), 7.21-7.26 (1H, m), 7.48-7.43 (1H, m).
With bis-triphenylphosphine-palladium(II) chloride; potassium carbonate; In tetrahydrofuran; water; for 3.0h;Inert atmosphere; Reflux; 1-Bromo-3,5-dichloro-2-fluorobenzene (10 g), (3,3,3-trifluoroprop-1-en-2-yl)-boronic acid (7.5 g:) andpotassium carbonate (13.6 g) were dissolved in tetrahydrofuran (41 ml) and water (20 ml), and then deaerated. Dichlorobis(triphenylphosphine)palladium (II) (1.4 g) was added thereto and the mixture was stirred for 3 hours under reflux under argon atomosphere. After cooling the mixture to the room temperature, water and n-hexane were added, and the organic layer was washed with water and dried over anhydrous magnesium sulfate. The drying agent was filtered off, the solvent was distilled off underreduced pressure, and the residue was roughly purified by silica gel chromatography (n-hexane) to obtain a mixture containing 1,3-dichloro-2,4-difluoro-5-(3,3,3-trifluoroprop-1-en-2-yl)benzene and hexane. 1H-NMR (CDCl3) 5: 5.82 (1H, s), 6.25 (1H, s), 7.21-7.26 (1H, m), 7.48-7.43 (1H, m).
  • 2
  • [ 1160573-64-7 ]
  • [ 1364674-31-6 ]
  • 3
  • [ 1160573-64-7 ]
  • 3-(3,5-dichloro-4-fluoro-phenyl)-3-trifluoromethyl-pyrrolidine [ No CAS ]
  • 4
  • [ 1160573-64-7 ]
  • 4-[3-(3,5-dichloro-4-fluorophenyl)-3-(trifluoromethyl)pyrrolidin-1-yl]-2-(trifluoromethyl)benzonitrile [ No CAS ]
  • 5
  • [ 1160573-64-7 ]
  • [ 1364674-34-9 ]
  • 6
  • [ 1160573-64-7 ]
  • [ 1364674-35-0 ]
  • 7
  • [ 1160573-64-7 ]
  • [ 1364674-32-7 ]
 

Historical Records

Technical Information

Categories

Related Functional Groups of
[ 1160573-64-7 ]

Fluorinated Building Blocks

Chemical Structure| 24812-13-3

A645092 [24812-13-3]

1-Bromo-3,5-dichloro-2,4,6-trifluorobenzene

Similarity: 0.97

Chemical Structure| 144584-65-6

A126022 [144584-65-6]

1-Bromo-3-chloro-2-fluorobenzene

Similarity: 0.97

Chemical Structure| 914636-89-8

A180553 [914636-89-8]

1-Bromo-5-chloro-2,4-difluorobenzene

Similarity: 0.94

Chemical Structure| 229180-34-1

A918789 [229180-34-1]

2-Bromo-4-chloro-1,3-difluorobenzene

Similarity: 0.94

Chemical Structure| 201849-13-0

A279146 [201849-13-0]

1-Bromo-3-chloro-2,4-difluorobenzene

Similarity: 0.94

Aryls

Chemical Structure| 24812-13-3

A645092 [24812-13-3]

1-Bromo-3,5-dichloro-2,4,6-trifluorobenzene

Similarity: 0.97

Chemical Structure| 144584-65-6

A126022 [144584-65-6]

1-Bromo-3-chloro-2-fluorobenzene

Similarity: 0.97

Chemical Structure| 914636-89-8

A180553 [914636-89-8]

1-Bromo-5-chloro-2,4-difluorobenzene

Similarity: 0.94

Chemical Structure| 201849-13-0

A279146 [201849-13-0]

1-Bromo-3-chloro-2,4-difluorobenzene

Similarity: 0.94

Chemical Structure| 229180-34-1

A918789 [229180-34-1]

2-Bromo-4-chloro-1,3-difluorobenzene

Similarity: 0.94

Bromides

Chemical Structure| 24812-13-3

A645092 [24812-13-3]

1-Bromo-3,5-dichloro-2,4,6-trifluorobenzene

Similarity: 0.97

Chemical Structure| 144584-65-6

A126022 [144584-65-6]

1-Bromo-3-chloro-2-fluorobenzene

Similarity: 0.97

Chemical Structure| 914636-89-8

A180553 [914636-89-8]

1-Bromo-5-chloro-2,4-difluorobenzene

Similarity: 0.94

Chemical Structure| 229180-34-1

A918789 [229180-34-1]

2-Bromo-4-chloro-1,3-difluorobenzene

Similarity: 0.94

Chemical Structure| 201849-13-0

A279146 [201849-13-0]

1-Bromo-3-chloro-2,4-difluorobenzene

Similarity: 0.94

Chlorides

Chemical Structure| 24812-13-3

A645092 [24812-13-3]

1-Bromo-3,5-dichloro-2,4,6-trifluorobenzene

Similarity: 0.97

Chemical Structure| 144584-65-6

A126022 [144584-65-6]

1-Bromo-3-chloro-2-fluorobenzene

Similarity: 0.97

Chemical Structure| 914636-89-8

A180553 [914636-89-8]

1-Bromo-5-chloro-2,4-difluorobenzene

Similarity: 0.94

Chemical Structure| 229180-34-1

A918789 [229180-34-1]

2-Bromo-4-chloro-1,3-difluorobenzene

Similarity: 0.94

Chemical Structure| 201849-13-0

A279146 [201849-13-0]

1-Bromo-3-chloro-2,4-difluorobenzene

Similarity: 0.94