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Chemical Structure| 116195-81-4 Chemical Structure| 116195-81-4

Structure of 116195-81-4

Chemical Structure| 116195-81-4

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Product Details of [ 116195-81-4 ]

CAS No. :116195-81-4
Formula : C5H3I2N
M.W : 330.89
SMILES Code : IC1=CN=C(I)C=C1
MDL No. :MFCD00234028
InChI Key :YHWFCFIXXMXRBF-UHFFFAOYSA-N
Pubchem ID :4245240

Safety of [ 116195-81-4 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 116195-81-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 116195-81-4 ]

[ 116195-81-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 116195-81-4 ]
  • [ 124-41-4 ]
  • [ 13472-61-2 ]
YieldReaction ConditionsOperation in experiment
82.7% In methanol; at 40℃; for 36h; A solution of the formula A-4 (80 g), sodium methoxide in methanol (30%, 60 g) was placed in a reaction vessel, and the reaction mixture was stirred and heated to about 40 C, and stirring was continued for 36 hours.After the reaction mixture was cooled to room temperature, the solvent was removed, ethyl acetate and water were added to extract, and the organic phase was dried, filtered, and the solvent was evaporated, and purified by distillation under reduced pressure to give the compound of formula B-4 (47 g, yield 82.7%).
 

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