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Chemical Structure| 117500-61-5 Chemical Structure| 117500-61-5

Structure of 117500-61-5

Chemical Structure| 117500-61-5

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Product Details of [ 117500-61-5 ]

CAS No. :117500-61-5
Formula : C9H11Cl2NO
M.W : 220.10
SMILES Code : O=C(Cl)C1=CC=CC(N(C)C)=C1.[H]Cl
MDL No. :MFCD19442144
Boiling Point : No data available
InChI Key :NUDQPATXNFWFNK-UHFFFAOYSA-N
Pubchem ID :22732309

Safety of [ 117500-61-5 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H302-H312-H314-H332
Precautionary Statements:P260-P261-P264-P270-P271-P280-P301+P312-P301+P330+P331-P302+P352-P303+P361+P353-P304+P340-P305+P351+P338-P310-P312-P321-P322-P330-P363-P405-P501
Class:8
UN#:3261
Packing Group:

Application In Synthesis of [ 117500-61-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 117500-61-5 ]

[ 117500-61-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 117500-61-5 ]
  • [ 5131-60-2 ]
  • [ 263400-73-3 ]
YieldReaction ConditionsOperation in experiment
With triethylamine; In dichloromethane; The N-(3-amino-4-chlorophenyl)-3-dimethylaminobenzamide used as a starting material was prepared as follows: A solution of 3-dimethylaminobenzoyl chloride hydrochloride (20 g) in methylene chloride (100 ml) was added dropwise over 2 hours to a solution of 4-chloro-3-aminoaniline (14.25 g) and triethylamine (38 ml) in methylene chloride (500 ml), and the reaction stirred at ambient temperature for 18 hours. The precipitated solid was collected to give the title compound (29.7 g, quantitative): NMR: 2.94 (s, 3H), 5.28 (s, 2H), 6.88 (m, 2H), 7.09 (d, 1H), 7.16 (m, 2H), 7.28 (dd, 1H), 7.33 (m, 1H), 9.91 (s, 1H); m/s 290, 292.
 

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