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Chemical Structure| 1187992-93-3 Chemical Structure| 1187992-93-3

Structure of 1187992-93-3

Chemical Structure| 1187992-93-3

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Product Details of [ 1187992-93-3 ]

CAS No. :1187992-93-3
Formula : C9H6N4O3
M.W : 218.17
SMILES Code : O=C(C1=CN=C(C2=NN=CC=C2)N=C1O)O

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Application In Synthesis of [ 1187992-93-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1187992-93-3 ]

[ 1187992-93-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1187992-93-3 ]
  • [ 19293-62-0 ]
  • [ 1187990-87-9 ]
YieldReaction ConditionsOperation in experiment
To a suspension of Intermediate 8 (14.94 g, 68.5 mmol) in DMF (225 mL) was added TEA (18.98 mL, 137 mmol) and CDI (11.10 g, 68.5 mmol). The reaction was heated at 120 C. for 1 h followed by the addition of 4,4'-dimethoxybenzhydrlamine (14.99 g, 61.6 mmol). The reaction was heated at 115 C. for 1 h, diluted with CHCl3, washed with aq. HCl (1 M), deionized H2O and concentrated. The material was crystallized from the residue using EtOH to afford the title compound. HPLC/MS: 444.18 (M+1); Rt=2.90 min.
 

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