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Structure of 1216936-29-6

Chemical Structure| 1216936-29-6

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Product Details of [ 1216936-29-6 ]

CAS No. :1216936-29-6
Formula : C12H22N2O2
M.W : 226.32
SMILES Code : CC(C)(C)OC(=O)N1CCC11CCNCC1
MDL No. :MFCD14581196
InChI Key :YQZFKXWWUMMHAH-UHFFFAOYSA-N
Pubchem ID :56962151

Safety of [ 1216936-29-6 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 1216936-29-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1216936-29-6 ]

[ 1216936-29-6 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 1216936-29-6 ]
  • [ 454-16-0 ]
  • tert-butyl 7-(2-methoxy-4-nitrophenyl)-1,7-diazaspiro[3.5]nonane-1-carboxylate [ No CAS ]
YieldReaction ConditionsOperation in experiment
With potassium carbonate; In N,N-dimethyl acetamide; at 120℃; tert- Butyl 1 ,7-diazaspiro[3.5]nonane-1-carboxylate (commercial, 300 mg, 1.33 mmol) was dissolved in DMA (5 ml_) and <strong>[454-16-0]1-fluoro-2-methoxy-4-nitrobenzene</strong> (227 mg, 1.33 mmol) was added followed by potassium carbonate (916 mg, 6.63 mmol). The suspension was heated to 120C and stirred overnight before cooling to RT and diluting with EtOAc. The organic phase was washed with 1 x water and 3 x 50% saturated brine solution and dried (anh. MgS04) and concentrated in vacuo to give the crude product (546 mg, 99%) as a yellow solid which was taken on as such into the next step. LCMS (Method B): RT = 1.55 min, m/z = 379 [M+H]+.
  • 2
  • [ 1216936-29-6 ]
  • [ 454-16-0 ]
  • tert-butyl 7-(4-amino-2-methoxyphenyl)-1,7-diazaspiro[3.5]nonane-1-carboxylate [ No CAS ]
 

Historical Records

Technical Information

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Related Functional Groups of
[ 1216936-29-6 ]

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Related Parent Nucleus of
[ 1216936-29-6 ]

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Spiroes

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