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Chemical Structure| 1218997-22-8 Chemical Structure| 1218997-22-8

Structure of 1218997-22-8

Chemical Structure| 1218997-22-8

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Product Details of [ 1218997-22-8 ]

CAS No. :1218997-22-8
Formula : C6H8BrN3
M.W : 202.05
SMILES Code : NC1=C(NC)C=NC(Br)=C1
MDL No. :MFCD27942281

Safety of [ 1218997-22-8 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H314
Precautionary Statements:P280-P305+P351+P338-P310
Class:8
UN#:2735
Packing Group:

Application In Synthesis of [ 1218997-22-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1218997-22-8 ]

[ 1218997-22-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 37718-11-9 ]
  • [ 1218997-22-8 ]
  • [ 1612172-01-6 ]
YieldReaction ConditionsOperation in experiment
93% With polyphosphoric acid; at 200℃; for 5h;Sealed tube; A mixture of 6-bromo-N -methylpyridine-3,4-diamine (54 mg, 0.27 mmol), lH-pyrazole-4- carboxylic acid (30 mg, 0.27 mmol) and polyphosphoric acid (0.5 mL) was heated at 200 °C in a sealed tube for 5 h. After cooling, the reaction mixture was diluted with water and taken to pH 7 by addition of 50percent> aq. NaOH. A white suspension formed and the solid was collected by filtration affording the title compound (69 mg, 93percent). LCMS (ESI): [M+H]+ 278.2.
 

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