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Chemical Structure| 1221237-83-7 Chemical Structure| 1221237-83-7

Structure of 1221237-83-7

Chemical Structure| 1221237-83-7

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Product Details of [ 1221237-83-7 ]

CAS No. :1221237-83-7
Formula : C22H13Br2N
M.W : 451.15
SMILES Code : BrC1=CC2=C(N(C3=CC=C4C=CC=CC4=C3)C5=C2C=C(Br)C=C5)C=C1
MDL No. :MFCD29072769
InChI Key :ZPMPPIIUVAZBBQ-UHFFFAOYSA-N
Pubchem ID :58384088

Safety of [ 1221237-83-7 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319
Precautionary Statements:P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313

Application In Synthesis of [ 1221237-83-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1221237-83-7 ]

[ 1221237-83-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1221237-83-7 ]
  • [ 439090-73-0 ]
  • C48H29N3O2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
80% With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In tetrahydrofuran; water; for 8.0h;Reflux; After the compound of Chemical Formula A (10 g,31.1 mmol) and 2,6-dibromo-N-(2-naphthyl)carbazole (7.0 g, 15.6 mmol) were suspension stirred in THF (310 ml), K2C03 (8.6 g, 62.3 mmol) dissolved in H20 (100 ml), and then tetrakis(triphenylphosphine) palladium(0) (720 mg, 0.62 mmol) were added thereto, and the result was refluxed for 8 hours. After the reaction was complete, the temperature was lowered to room temperature, the water layer was removed, and the organic layer was treated with magnesium sulfate (MgSO4) and then filtered. The solution was vacuum concentrated under reduced pressure, and column purified with a ratio of THF/Hexane=1/2 to obtain a compound of Chemical Formula 1-51 (8.7 g, yield: 80%).MS: [M+H]=680
 

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