Home Cart Sign in  
Chemical Structure| 122321-03-3 Chemical Structure| 122321-03-3

Structure of 122321-03-3

Chemical Structure| 122321-03-3

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 122321-03-3 ]

CAS No. :122321-03-3
Formula : C15H16N2O2
M.W : 256.30
SMILES Code : O=CC1=CC=C(OCCN(C)C2=NC=CC=C2)C=C1
MDL No. :MFCD09751241

Safety of [ 122321-03-3 ]

Application In Synthesis of [ 122321-03-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 122321-03-3 ]

[ 122321-03-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 6972-82-3 ]
  • [ 122321-03-3 ]
  • 3-methyl-8-(4-(2-(methyl(pyridin-2-yl)amino)ethoxy)phenyl)-1H-purine-2,6 (3H,7H)-dione [ No CAS ]
YieldReaction ConditionsOperation in experiment
General procedure: A mixture of compound 9 or compound 12 (4.8 mmol), compound 3 (5.3 mmol) and 1.5mL of acetic acid was refluxed for 4 h in 20 mL of ethanol. Upon cooling of the mixture, the precipitate was filtered and washed with ethanol then diethyl ether to give the Schiff-base, which was used directly in the next step. Schiff-base (3.3 mmol) was heated in 20 mL of toluene. As the mixture began to reflux, diisopropyl azodicarboxylate (6.5 mmol) was added through the condenser. After another 2 h, the reaction mixture was filtered, and the precipitate was washed with ethanol and diethylether to give compound 10 and 13.
 

Historical Records

Technical Information

Categories