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[ CAS No. 124931-12-0 ] {[proInfo.proName]}

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Chemical Structure| 124931-12-0
Chemical Structure| 124931-12-0
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Product Details of [ 124931-12-0 ]

CAS No. :124931-12-0 MDL No. :MFCD00134233
Formula : C8H18NO5P Boiling Point : No data available
Linear Structure Formula :- InChI Key :WYLRYBDGIILFIR-UHFFFAOYSA-N
M.W : 239.21 Pubchem ID :2773719
Synonyms :

Safety of [ 124931-12-0 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P305+P351+P338 UN#:
Hazard Statements:H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 124931-12-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 124931-12-0 ]

[ 124931-12-0 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 67442-07-3 ]
  • [ 122-52-1 ]
  • [ 124931-12-0 ]
YieldReaction ConditionsOperation in experiment
78% at 100℃; for 18h; A solution of <strong>[67442-07-3]2-chloro-N-methoxy-N-methylacetamide</strong> (2.48 g,17.7 mmol) and triethyl phosphite (3.00 mL, 17.7 mmol) was heated to 100 °C for 18 h. The crude product was purified by flash column chromatography (0?2percent MeOH in CH2Cl2) to give 1 as a colorless oil; yield: 3.31 g (13.8 mmol; 78percent); Rf = 0.42 (2percent MeOH in CH2Cl2); HPLC purity (method b): >95percent (210 nm), >95percent (254 nm). IR (ATR): 2985, 2940, 2908, 1659, 1381, 1253, 1050, 1020, 998, 961 cm?1. 1H NMR (400 MHz, CDCl3): delta = 4.26?4.07 (m, 4 H, 2 × OCH2CH3), 3.76(s, 3 H, OCH3), 3.20 (s, 3 H, NCH3), 3.15 (d, J = 22.1 Hz, 2 H, 1-H), 1.33(td, J = 7.1, 0.6 Hz, 6 H, 2 × OCH2CH3). 13C NMR (101 MHz, CDCl3): delta = 166.2 (C-2), 62.7 (2 × OCH2CH3), 61.6(OCH3), 32.3 (NCH3), 30.9 (C-1), 16.5 (2 × OCH2CH3). HRMS (ESI): m/z [M + H]+ calcd for C8H19NO5P+: 240.0995; found: 240.0996.
  • 2
  • [ 762-04-9 ]
  • [ 67442-07-3 ]
  • [ 124931-12-0 ]
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