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Chemical Structure| 1263199-75-2 Chemical Structure| 1263199-75-2

Structure of 1263199-75-2

Chemical Structure| 1263199-75-2

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Product Details of [ 1263199-75-2 ]

CAS No. :1263199-75-2
Formula : C5H8O5S
M.W : 180.18
SMILES Code : O=C(OC1COS(=O)(=O)C1)C
MDL No. :N/A

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Application In Synthesis of [ 1263199-75-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1263199-75-2 ]

[ 1263199-75-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1263199-75-2 ]
  • [ 21806-61-1 ]
YieldReaction ConditionsOperation in experiment
66% With potassium carbonate; In water; ethyl acetate; at 40℃; for 12h; Example 6Synthesis of 1,3-propenesultone (a step to obtain the compound represented by the general formula [4] from the compound represented by the general formula [5] in the third step, Reaction Scheme [VII])2-Acetoxy-1,3-propanesultone (0.50 g, 2.78 mmol) divided from the total amount thereof obtained in Example 5 was dissolved in ethyl acetate (5 mL), and thereafter a solution of potassium carbonate (0.23 g, 1.66 mmol, produced by Wako Pure Chemical Industries, Ltd.) in water (5 mL) was added thereto. The solution was stirred at 40 C. for 12 hours to promote the reaction. After completion of the reaction, the reaction solution was washed with water, and then the organic layer was separated. After the separated organic layer was concentrated, to obtain 1,3-propenesultone (0.22 g, yield: 66%) relevant to the above-described general formula [4] as a white crystal.
 

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