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Chemical Structure| 130193-90-7 Chemical Structure| 130193-90-7

Structure of 130193-90-7

Chemical Structure| 130193-90-7

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Product Details of [ 130193-90-7 ]

CAS No. :130193-90-7
Formula : C12H14O3
M.W : 206.24
SMILES Code : O=C([C@@H]1COCC1)OCC2=CC=CC=C2

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Application In Synthesis of [ 130193-90-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 130193-90-7 ]

[ 130193-90-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 130193-90-7 ]
  • [ 168395-26-4 ]
YieldReaction ConditionsOperation in experiment
With palladium on activated charcoal; hydrogen; In ethanol; at 20℃; for 18h; c) (S)-Tetrahydro-furan-3-carboxylic acid/(R)-Tetrahydro-furan-3-carboxylic acidA solution of an enantiomerically pure tetrahydro-furan-3-carboxylic acid benzyl ester (peak 1 or peak 2, 200 mg, 0.97 mmol), Pd/C (103 mg, 0.97 mmol) in EtOH (2 ml) was hydrogenated with H2 at rt for 18 h. Filtration of the reaction mixture and concentration of the filtrate afforded the title compound as colourless oil (125 mg (Peak 1), 111 mg (Peak 2), crude). [0808] 1H NMR (both enantiomers) (400 MHz, DMSO-d6): δ 12.40 (br s, 1H), 3.84-3.59 (m, 4H), 3.00 (m, 1H), 2.08-1.92 (m, 1H).
 

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