Home Cart 0 Sign in  

[ CAS No. 130277-32-6 ] {[proInfo.proName]}

,{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]}
Chemical Structure| 130277-32-6
Chemical Structure| 130277-32-6
Structure of 130277-32-6 * Storage: {[proInfo.prStorage]}
Cart0 Add to My Favorites Add to My Favorites Bulk Inquiry Inquiry Add To Cart

Quality Control of [ 130277-32-6 ]

Related Doc. of [ 130277-32-6 ]

Alternatived Products of [ 130277-32-6 ]
Product Citations

Product Details of [ 130277-32-6 ]

CAS No. :130277-32-6 MDL No. :MFCD15529614
Formula : C21H26O3Si Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 354.51 Pubchem ID :-
Synonyms :

Safety of [ 130277-32-6 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 130277-32-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 130277-32-6 ]

[ 130277-32-6 ] Synthesis Path-Downstream   1~6

  • 1
  • [ 1445-39-2 ]
  • [ 130277-32-6 ]
  • [ 307303-59-9 ]
  • 2
  • [ 130277-32-6 ]
  • [ 181871-83-0 ]
  • [ 503321-53-7 ]
  • 3
  • [ 130277-32-6 ]
  • [ 68050-37-3 ]
  • (2'R)-cis-5-[2',5'-dihydro-4'-(tert-butyldiphenylsilyl)oxy-2'-furanyl]-2-aminoquinoline [ No CAS ]
  • 4
  • [ 884660-47-3 ]
  • [ 130277-32-6 ]
  • [(2R,5R)-5-(6-Amino-2-fluoro-pyridin-3-yl)-3-(tert-butyl-diphenyl-silanyloxy)-2,5-dihydro-furan-2-yl]-methanol [ No CAS ]
YieldReaction ConditionsOperation in experiment
With tris(dibenzylideneacetone)palladium; N-ethyl-N,N-diisopropylamine; tris(pentafluorophenyl)phosphine In acetonitrile at 55℃; for 48h;
  • 5
  • [ 130277-32-6 ]
  • [ 75073-11-9 ]
  • [(2R,5R)-5-(6-Amino-2-methyl-pyridin-3-yl)-3-(tert-butyl-diphenyl-silanyloxy)-2,5-dihydro-furan-2-yl]-methanol [ No CAS ]
  • 6
  • [ 130277-32-6 ]
  • [ 790692-90-9 ]
  • C26H28ClN3O5Si [ No CAS ]
YieldReaction ConditionsOperation in experiment
63% A solution of palladium acetate (187 mg, 0.83 mmol) and triphenyl arsine (509 mg, 1.66 mmol) in chloroform (30 mL) was stirred for 30 min at room temperature. This solution was added to the mixture of glycal (3.25 g, 9.2 mmol), 2 (2.49 g, 8.3 mmol) and silver carbonate (4.59 g, 16.6 mmol) in chloroform (60 mL) at room temperature. The reaction mixture was refluxed overnight, cooled to room temperature and filtered through a celite pad, the filtrate was concentrated and the residue was purified by silica gel column chromatography (Hex/EtOAc=4/1 to 7/3) to give compound 3 (2.75 g, 5.23 mmol, 63%) as an orange foam. 1H NMR (CDCl3, 300 MHz) delta8.42 (s, 1H), 7.73-7.82 (m, 4H), 7.41-7.48 (m, 6H), 5.83 (nm, 1H), 7.77 (m, 1H), 4.23 (s, 1H), 3.90 (m, 2H), 1.78 (t, 1H, J=6.0), 1.23 (t, 1H, J=6.9), 1.08 (s, 9H).
Recommend Products
Same Skeleton Products
Historical Records