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Structure of 13080-75-6

Chemical Structure| 13080-75-6

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Product Details of [ 13080-75-6 ]

CAS No. :13080-75-6
Formula : C16H15NO
M.W : 237.30
SMILES Code : CC(N1C2=CC=CC=C2CCC3=CC=CC=C31)=O
MDL No. :MFCD00191704
InChI Key :QBSUAHGUFKVVTM-UHFFFAOYSA-N
Pubchem ID :735931

Safety of [ 13080-75-6 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302
Precautionary Statements:P301+P312+P330

Application In Synthesis of [ 13080-75-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 13080-75-6 ]

[ 13080-75-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 13080-75-6 ]
  • [ 25961-11-9 ]
YieldReaction ConditionsOperation in experiment
90% With bis(trichloromethyl) carbonate; tetrabutylammomium bromide; potassium carbonate; In dichloromethane; at 0 - 10℃; for 5h; In 500ml reaction flask was added N-dibenzylamino-acetyl imino (II) (23.73g, 100mmol), potassium carbonate (13.82,100mmol), tetrabutylammonium bromide (2.78g, 10mmol), 100mL dichloroethane after mixing evenly, cooled to 0 deg.] C, and then added dropwise to the system bis(trichloromethyl)carbonate (38.58g, 130mmol), dropwise after the temperature was raised to 10 C, the reaction incubated for 5 hours. Concentrated under atmosphere pressure to dryness to give the desired product as a pale yellow oily substance acetyl-3-chloro-N-iminodibenzyl (I) 24.45g, 90.0% yield.
 

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