Home Cart Sign in  
HazMat Fee +

There will be a HazMat fee per item when shipping a dangerous goods. The HazMat fee will be charged to your UPS/DHL/FedEx collect account or added to the invoice unless the package is shipped via Ground service. Ship by air in Excepted Quantity (each bottle), which is up to 1g/1mL for class 6.1 packing group I or II, and up to 25g/25ml for all other HazMat items.

Type HazMat fee for 500 gram (Estimated)
Excepted Quantity USD 0.00
Limited Quantity USD 15-60
Inaccessible (Haz class 6.1), Domestic USD 80+
Inaccessible (Haz class 6.1), International USD 150+
Accessible (Haz class 3, 4, 5 or 8), Domestic USD 100+
Accessible (Haz class 3, 4, 5 or 8), International USD 200+
Chemical Structure| 13105-72-1 Chemical Structure| 13105-72-1

Structure of 13105-72-1

Chemical Structure| 13105-72-1

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 13105-72-1 ]

CAS No. :13105-72-1
Formula : C6H11NO
M.W : 113.16
SMILES Code : C#CCN(CCO)C
MDL No. :MFCD14631477
InChI Key :FKPAVGPHHCZBEB-UHFFFAOYSA-N
Pubchem ID :287929

Safety of [ 13105-72-1 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H302-H335-H314-H227
Precautionary Statements:P210-P260-P264-P270-P271-P280-P301+P330+P331-P303+P361+P353-P304+P340-P305+P351+P338-P310-P363-P370+P378-P403+P233-P403+P235-P405-P501
Class:8
UN#:2735
Packing Group:

Application In Synthesis of [ 13105-72-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 13105-72-1 ]

[ 13105-72-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 53595-65-6 ]
  • [ 13105-72-1 ]
  • 5-{3-[2-hydroxyethyl(methyl)amino]prop-1-yn-1-yl}thiophene-2-sulfonamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
69% With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In ethyl acetate; at 50℃; for 1h;Inert atmosphere; General procedure: Pd(PPh3)2Cl2 (26.2 mg, 0.1 mmol) and CuI (9.5 mg,0.05 mmol) were added to triethylamine (1 ml) under argonatmosphere and stirred for 5 min. Then a solution of5-bromo-2-thiophene sulfonamide (1) (242 mg, 1 mmol) inEtOAc (5 ml) and the appropriate tertiary propargylamine(2 mmol) were added. The reaction mixture was stirred for1 h at 50 under inert atmosphere. The reaction mixturewas then cooled, diluted with EtOAc, and treated with a fewdrops of aqueous ammonia, stirred for 5-10 min and filteredthrough a thin layer of silica gel. The solution was evaporatedto dryness and the product was isolated by silica gel columnchromatography (eluent CH2Cl2-EtOAc-MeOH). In order toobtain hydrochlorides, the isolated product was dissolvedin 1:1 EtOAc-Et2O mixture and treated with anhydrousethereal HCl solution to pH 1. The mixture was stirred untilthe reaction was complete (TLC control), evaporated todryness, and diluted with anhydrous ether. The precipitatewas collected by filtration and dried.
 

Historical Records

Technical Information

Categories