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Chemical Structure| 1361215-96-4 Chemical Structure| 1361215-96-4

Structure of 1361215-96-4

Chemical Structure| 1361215-96-4

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Product Details of [ 1361215-96-4 ]

CAS No. :1361215-96-4
Formula : C18H21BO4S
M.W : 344.23
SMILES Code : O=S(C1=CC=C(B2OC(C)(C)C(C)(C)O2)C=C1)(C3=CC=CC=C3)=O
MDL No. :MFCD31641436

Safety of [ 1361215-96-4 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319
Precautionary Statements:P501-P270-P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313-P301+P312+P330

Application In Synthesis of [ 1361215-96-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1361215-96-4 ]

[ 1361215-96-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1361215-96-4 ]
  • [ 57103-20-5 ]
  • 9-phenyl-3,6-bis[(4-phenylsulfone-yl)phenyl]-9H-carbazole [ No CAS ]
YieldReaction ConditionsOperation in experiment
45.21% With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In ethanol; water; toluene; for 24h;Reflux; Inert atmosphere; Example 2:Preparation of compounds of formula 4 500ml three-necked flask,Obtained above, a compound of Formula 2 6.05g (17.6mmol),<strong>[57103-20-5]3,6-dibromo-9-phenyl-carbazole</strong> 3.28g (8mmol),Tetrakis (triphenylphosphine) palladium 1.0g,20ml aqueous potassium carbonate (4.3g of potassium carbonate dissolved in 20ml of water),40ml and 200ml of toluene ethanol mix,Reflux under nitrogen for 24h.The reaction was cooled to room temperature,Then extracted with dichloromethane (2 * 200ml),The combined organic layersDried over anhydrous sodium sulfate,Concentrated to give an oil.After column chromatography,Volume ratio of ethyl acetate: petroleum ether = 1:10 ~ 1: 3 as eluentTo give a white solid 2.5g,Yield 45.21percent.
 

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