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Chemical Structure| 14068-53-2 Chemical Structure| 14068-53-2

Structure of 14068-53-2

Chemical Structure| 14068-53-2

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Product Details of [ 14068-53-2 ]

CAS No. :14068-53-2
Formula : C4H7N3S
M.W : 129.18
SMILES Code : NC1=NN=C(CC)S1
MDL No. :MFCD00003111
InChI Key :QXTRPGAMVIONMK-UHFFFAOYSA-N
Pubchem ID :26444

Safety of [ 14068-53-2 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 14068-53-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 14068-53-2 ]

[ 14068-53-2 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 14068-53-2 ]
  • [ 58755-91-2 ]
  • [ 139477-32-0 ]
  • 2
  • [ 14068-53-2 ]
  • [ 437-86-5 ]
  • [ 1420066-27-8 ]
YieldReaction ConditionsOperation in experiment
15% With N-ethyl-N,N-diisopropylamine; In 1-methyl-pyrrolidin-2-one; at 140℃; for 16h;Sealed tube; General procedure: A mixture of 1 (1.55 mmol, unless otherwise stated), 2 (0.77 mmol), and i-Pr2NEt (1.55 mmol) in NMP (0.77 mL) was stirred at 140 °C in a sealed tube for 16 h. The mixture was allowed to cool to room temperature, diluted (DCM), washed (satd Na2CO3), dried (filtered through a Biotage® phase separator), and concentrated. Purification method A: the residue was purifiedby reverse phase automated preparative HPLC. Purification method B: the residue was purified by flash column chromatography (SiO2).
 

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